(2S,2'R,5'S)-5'-[(R)-1-(tert-butyldimethylsilyloxy)ethyl]-5-{[(4S,5S,6R)-6-[(R)-1-(tert-butyldiphenylsilyloxy)propan-2-yl]-2,2,5-trimethyl-1,3-dioxan-4-yl]methyl}-2,5'-dimethyl-octahydro-2,2'-bifuran

Base Information

Chemical Name:(2S,2'R,5'S)-5'-[(R)-1-(tert-butyldimethylsilyloxy)ethyl]-5-{[(4S,5S,6R)-6-[(R)-1-(tert-butyldiphenylsilyloxy)propan-2-yl]-2,2,5-trimethyl-1,3-dioxan-4-yl]methyl}-2,5'-dimethyl-octahydro-2,2'-bifuran
CAS No.:1184871-27-9
Molecular Formula:C₄₅H₇₄O₆Si₂
Molecular Weight:767.25
Hs Code.:

(2S,2'R,5'S)-5'-[(R)-1-(tert-butyldimethylsilyloxy)ethyl]-5-{[(4S,5S,6R)-6-[(R)-1-(tert-butyldiphenylsilyloxy)propan-2-yl]-2,2,5-trimethyl-1,3-dioxan-4-yl]methyl}-2,5'-dimethyl-octahydro-2,2'-bifuran

Synonyms:(2S,2'R,5'S)-5'-[(R)-1-(tert-butyldimethylsilyloxy)ethyl]-5-{[(4S,5S,6R)-6-[(R)-1-(tert-butyldiphenylsilyloxy)propan-2-yl]-2,2,5-trimethyl-1,3-dioxan-4-yl]methyl}-2,5'-dimethyl-octahydro-2,2'-bifuran

Suppliers and Price of (2S,2'R,5'S)-5'-[(R)-1-(tert-butyldimethylsilyloxy)ethyl]-5-{[(4S,5S,6R)-6-[(R)-1-(tert-butyldiphenylsilyloxy)propan-2-yl]-2,2,5-trimethyl-1,3-dioxan-4-yl]methyl}-2,5'-dimethyl-octahydro-2,2'-bifuran

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S,2'R,5'S)-5'-[(R)-1-(tert-butyldimethylsilyloxy)ethyl]-5-{[(4S,5S,6R)-6-[(R)-1-(tert-butyldiphenylsilyloxy)propan-2-yl]-2,2,5-trimethyl-1,3-dioxan-4-yl]methyl}-2,5'-dimethyl-octahydro-2,2'-bifuran

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S,2'R,5'S)-5'-[(R)-1-(tert-butyldimethylsilyloxy)ethyl]-5-{[(4S,5S,6R)-6-[(R)-1-(tert-butyldiphenylsilyloxy)propan-2-yl]-2,2,5-trimethyl-1,3-dioxan-4-yl]methyl}-2,5'-dimethyl-octahydro-2,2'-bifuran

There total 1 articles about (2S,2'R,5'S)-5'-[(R)-1-(tert-butyldimethylsilyloxy)ethyl]-5-{[(4S,5S,6R)-6-[(R)-1-(tert-butyldiphenylsilyloxy)propan-2-yl]-2,2,5-trimethyl-1,3-dioxan-4-yl]methyl}-2,5'-dimethyl-octahydro-2,2'-bifuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1184871-26-8
(3S,4R,5R)-3-{[(2S,2'R,5'S)-5'-[(R)-1-(tert-butyldimethylsilyloxy)ethyl]-2,5-dimethyl-octahydro-2,2'-bifuran-5-yl]methyl}-5-[(R)-1-(tert-butyldiphenylsilyloxy)propan-2-yl]-2,2,4-trimethyl-1,2-oxasilolane

: 77-76-9
2,2-dimethoxy-propane

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1184871-27-9
(2S,2'R,5'S)-5'-[(R)-1-(tert-butyldimethylsilyloxy)ethyl]-5-{[(4S,5S,6R)-6-[(R)-1-(tert-butyldiphenylsilyloxy)propan-2-yl]-2,2,5-trimethyl-1,3-dioxan-4-yl]methyl}-2,5'-dimethyl-octahydro-2,2'-bifuran

Guidance literature:: (3S,4R,5R)-3-{[(2S,2'R,5'S)-5'-[(R)-1-(tert-butyldimethylsilyloxy)ethyl]-2,5-dimethyl-octahydro-2,2'-bifuran-5-yl]methyl}-5-[(R)-1-(tert-butyldiphenylsilyloxy)propan-2-yl]-2,2,4-trimethyl-1,2-oxasilolane; With dihydrogen peroxide; potassium hydroxide; In water; N,N-dimethyl-formamide; at 20 ℃; for 2h;

tert-butylchlorodiphenylsilane; With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

2,2-dimethoxy-propane; With pyridinium p-toluenesulfonate; at 20 ℃; for 1h;
DOI:10.1002/anie.200901608