C₂₇H₂₄N₂O₉S₂

Base Information

Chemical Name:C₂₇H₂₄N₂O₉S₂
CAS No.:1093120-77-4
Molecular Formula:C₂₇H₂₄N₂O₉S₂
Molecular Weight:584.628
Hs Code.:

C<sub>27</sub>H<sub>24</sub>N<sub>2</sub>O<sub>9</sub>S<sub>2</sub>

Synonyms:C₂₇H₂₄N₂O₉S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₂₄N₂O₉S₂

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Technology Process of C₂₇H₂₄N₂O₉S₂

There total 7 articles about C₂₇H₂₄N₂O₉S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 1093121-27-7
C₃₄H₄₀N₂O₉S₂Si

: 1093120-77-4
C₂₇H₂₄N₂O₉S₂

Guidance literature:: C₃₄H₄₀N₂O₉S₂Si; With lithium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 12h;

With hydrogenchloride; In tetrahydrofuran; water; ethyl acetate; pH=2;

Reference yield:

: 752242-45-8
3-hydroxy-5-(4-methanesulfonylphenoxy)benzoic acid methyl ester

: 1093120-77-4
C₂₇H₂₄N₂O₉S₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 3.75 h / 0 - 20 °C

2.1: lithium hydroxide; water / tetrahydrofuran; methanol / 3 h / 20 °C

2.2: pH 4

3.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 72 h / 20 °C

4.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

5.1: benzotriazol-1-ol; triethylamine / dichloromethane / 0.17 h / 20 °C

5.2: 12 h / 20 °C

6.1: lithium hydroxide; water / tetrahydrofuran / 12 h / 20 °C

6.2: pH 2

With 1H-imidazole; lithium hydroxide; di-isopropyl azodicarboxylate; water; hydrogen; benzotriazol-1-ol; triethylamine; triphenylphosphine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1001419-67-5
3-[(1S)-2-benzyloxy-1-methylethoxy]-5-[4-(methylsulfonyl)phenoxy]benzoic acid

: 1093120-77-4
C₂₇H₂₄N₂O₉S₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 72 h / 20 °C

2.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

3.1: benzotriazol-1-ol; triethylamine / dichloromethane / 0.17 h / 20 °C

3.2: 12 h / 20 °C

4.1: lithium hydroxide; water / tetrahydrofuran / 12 h / 20 °C

4.2: pH 2

With 1H-imidazole; lithium hydroxide; water; hydrogen; benzotriazol-1-ol; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;