Phenethyl-Thiocarbamic Acid O-3-[4(t-butyl-dimethyl-silanyloxy)-3-methoxy-phenyl]-1-ethyl-propyl Ester

Base Information

Chemical Name:Phenethyl-Thiocarbamic Acid O-3-[4(t-butyl-dimethyl-silanyloxy)-3-methoxy-phenyl]-1-ethyl-propyl Ester
CAS No.:402469-25-4
Molecular Formula:C₂₇H₄₁NO₃SSi
Molecular Weight:487.779
Hs Code.:

Synonyms:Phenethyl-Thiocarbamic Acid O-3-[4(t-butyl-dimethyl-silanyloxy)-3-methoxy-phenyl]-1-ethyl-propyl Ester

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Chemical Property of Phenethyl-Thiocarbamic Acid O-3-[4(t-butyl-dimethyl-silanyloxy)-3-methoxy-phenyl]-1-ethyl-propyl Ester

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Technology Process of Phenethyl-Thiocarbamic Acid O-3-[4(t-butyl-dimethyl-silanyloxy)-3-methoxy-phenyl]-1-ethyl-propyl Ester

There total 5 articles about Phenethyl-Thiocarbamic Acid O-3-[4(t-butyl-dimethyl-silanyloxy)-3-methoxy-phenyl]-1-ethyl-propyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 458-36-6
trans-coniferyl aldehyde

: 402469-25-4
Phenethyl-Thiocarbamic Acid O-3-[4(t-butyl-dimethyl-silanyloxy)-3-methoxy-phenyl]-1-ethyl-propyl Ester

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / NaH / tetrahydrofuran

2: tetrahydrofuran

3: H₂ / Pd/C / methanol

4: NaH / tetrahydrofuran

With hydrogen; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1016/S0960-894X(03)00178-1

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 402469-25-4
Phenethyl-Thiocarbamic Acid O-3-[4(t-butyl-dimethyl-silanyloxy)-3-methoxy-phenyl]-1-ethyl-propyl Ester

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / NaH / tetrahydrofuran

2: tetrahydrofuran

3: H₂ / Pd/C / methanol

4: NaH / tetrahydrofuran

With hydrogen; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1016/S0960-894X(03)00178-1

Reference yield:

: 1-[4-(tert-butyl-dimethyl-silanyloxy)-3-methoxy-phenyl]-pent-1-en-3-ol

: 402469-25-4
Phenethyl-Thiocarbamic Acid O-3-[4(t-butyl-dimethyl-silanyloxy)-3-methoxy-phenyl]-1-ethyl-propyl Ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / methanol

2: NaH / tetrahydrofuran

With hydrogen; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1016/S0960-894X(03)00178-1