pentacarbonyl(N,N-diethyl-2-methyl-3,3-diphenylselenoacrylamide)chromium

Base Information

Chemical Name:pentacarbonyl(N,N-diethyl-2-methyl-3,3-diphenylselenoacrylamide)chromium
CAS No.:110657-72-2
Molecular Formula:C₂₅H₂₃CrNO₅Se
Molecular Weight:548.417
Hs Code.:

Synonyms:pentacarbonyl(N,N-diethyl-2-methyl-3,3-diphenylselenoacrylamide)chromium

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Chemical Property of pentacarbonyl(N,N-diethyl-2-methyl-3,3-diphenylselenoacrylamide)chromium

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Technology Process of pentacarbonyl(N,N-diethyl-2-methyl-3,3-diphenylselenoacrylamide)chromium

There total 1 articles about pentacarbonyl(N,N-diethyl-2-methyl-3,3-diphenylselenoacrylamide)chromium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 88676-87-3
(CO)5Cr(Se=CPh₂)

: 4231-35-0
methyl(diethylamino)acetylene

: 110657-72-2
pentacarbonyl(N,N-diethyl-2-methyl-3,3-diphenylselenoacrylamide)chromium

Guidance literature:: In dichloromethane; N2 atmosphere, addn. of MeCCNEt2 in CH2Cl2 (room temp.) to cooled (-78°C) soln. of complex, warming to room temp.; chromy. (silica gel, -25°C, pentane, pentane/CH2Cl2 3:1), solvent removal (high vacuum), recrystn. (pentane/CH2Cl2 5:1); elem. anal.;

Reference yield:

: 110657-72-2
pentacarbonyl(N,N-diethyl-2-methyl-3,3-diphenylselenoacrylamide)chromium

: 199620-14-9,13007-92-6
chromium⁽⁰⁾ hexacarbonyl

: 110789-82-7
N,N-Diethyl-2-methyl-3,3-diphenylselenoacrylamid

Guidance literature:: With carbon monoxide; In diethyl ether; a soln. of Cr complex in Et2O was reacted with CO (100 atm, 50°C) for 10-15 h;
DOI:10.1039/c39870000559