Technology Process of C29H36N6O5
There total 7 articles about C29H36N6O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C35H50N6O5Si;
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 20 ℃;
for 3h;
With
water;
In
tetrahydrofuran;
Cooling with ice;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: caesium carbonate / 1,2-dimethoxyethane; water / 1 h / 60 °C
1.2: 0.5 h / 60 °C
2.1: 1H-imidazole / dichloromethane / 20 °C / Inert atmosphere
3.1: caesium carbonate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,2-dimethoxyethane / 72 h / 85 °C / Inert atmosphere
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C
4.2: Cooling with ice
With
1H-imidazole; tetrabutyl ammonium fluoride; caesium carbonate;
palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl;
In
tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 - 5 °C / Inert atmosphere
1.2: 18 h / 5 - 20 °C / Inert atmosphere
2.1: caesium carbonate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,2-dimethoxyethane / 72 h / 85 °C / Inert atmosphere
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C
3.2: Cooling with ice
With
tetrabutyl ammonium fluoride; sodium hydride; caesium carbonate;
palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl;
In
tetrahydrofuran; 1,2-dimethoxyethane; N,N-dimethyl-formamide; mineral oil;
