2-tert-butoxycarbonylamino-8-(tert-butyl-diphenyl-silanyloxy)-decanoic acid

Base Information

Chemical Name:2-tert-butoxycarbonylamino-8-(tert-butyl-diphenyl-silanyloxy)-decanoic acid
CAS No.:330814-51-2
Molecular Formula:C₃₁H₄₇NO₅Si
Molecular Weight:541.803
Hs Code.:

2-<i>tert</i>-butoxycarbonylamino-8-(<i>tert</i>-butyl-diphenyl-silanyloxy)-decanoic acid

Synonyms:2-tert-butoxycarbonylamino-8-(tert-butyl-diphenyl-silanyloxy)-decanoic acid

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Chemical Property of 2-tert-butoxycarbonylamino-8-(tert-butyl-diphenyl-silanyloxy)-decanoic acid

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Technology Process of 2-tert-butoxycarbonylamino-8-(tert-butyl-diphenyl-silanyloxy)-decanoic acid

There total 8 articles about 2-tert-butoxycarbonylamino-8-(tert-butyl-diphenyl-silanyloxy)-decanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 98541-64-1
(S)-3-(tert-butoxycarbonylamino)-oxetan-2-one

: 330814-50-1
(5-bromo-1-ethyl-pentyloxy)-tert-butyl-diphenyl-silane

: 330814-51-2
2-tert-butoxycarbonylamino-8-(tert-butyl-diphenyl-silanyloxy)-decanoic acid

Guidance literature:: With copper(I) bromide dimethylsulfide complex; magnesium;
DOI:10.3987/com-00-9014

Reference yield:

: 83067-20-3
5-(tert-butyldimethyl-silyloxy)pentan-1-ol

: 330814-51-2
2-tert-butoxycarbonylamino-8-(tert-butyl-diphenyl-silanyloxy)-decanoic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 70 percent / PCC

2: 100 percent

3: 89 percent

4: 79 percent / TBAF

5: 59 percent / PPh₃; CBr₄

6: 35 percent / Mg; CuBr*SMe₂

With copper(I) bromide dimethylsulfide complex; carbon tetrabromide; tetrabutyl ammonium fluoride; magnesium; triphenylphosphine; pyridinium chlorochromate; 6: Grignard reaction;
DOI:10.3987/com-00-9014

Reference yield:

: 87184-80-3
5-tert-butyldimethylsilyloxypentanal

: 330814-51-2
2-tert-butoxycarbonylamino-8-(tert-butyl-diphenyl-silanyloxy)-decanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent

2: 89 percent

3: 79 percent / TBAF

4: 59 percent / PPh₃; CBr₄

5: 35 percent / Mg; CuBr*SMe₂

With copper(I) bromide dimethylsulfide complex; carbon tetrabromide; tetrabutyl ammonium fluoride; magnesium; triphenylphosphine; 5: Grignard reaction;
DOI:10.3987/com-00-9014