cyclopentyl (2S)-[(4-{[{[2,4-dihydroxy-5-(propan-2-yl)phenyl]carbonyl}(methyl)amino]methyl}benzyl)amino](phenyl)ethanoate

Base Information

Chemical Name:cyclopentyl (2S)-[(4-{[{[2,4-dihydroxy-5-(propan-2-yl)phenyl]carbonyl}(methyl)amino]methyl}benzyl)amino](phenyl)ethanoate
CAS No.:1351814-69-1
Molecular Formula:C₃₂H₃₈N₂O₅
Molecular Weight:530.664
Hs Code.:

Synonyms:cyclopentyl (2S)-[(4-{[{[2,4-dihydroxy-5-(propan-2-yl)phenyl]carbonyl}(methyl)amino]methyl}benzyl)amino](phenyl)ethanoate

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Chemical Property of cyclopentyl (2S)-[(4-{[{[2,4-dihydroxy-5-(propan-2-yl)phenyl]carbonyl}(methyl)amino]methyl}benzyl)amino](phenyl)ethanoate

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Technology Process of cyclopentyl (2S)-[(4-{[{[2,4-dihydroxy-5-(propan-2-yl)phenyl]carbonyl}(methyl)amino]methyl}benzyl)amino](phenyl)ethanoate

There total 12 articles about cyclopentyl (2S)-[(4-{[{[2,4-dihydroxy-5-(propan-2-yl)phenyl]carbonyl}(methyl)amino]methyl}benzyl)amino](phenyl)ethanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 1351815-73-0
cyclopentyl (2S)-[(4-{[{[2,4-bis(benzyloxy)-5-(prop-1-en-2-yl)phenyl]carbonyl}(methyl)amino]methyl}benzyl)amino](phenyl)ethanoate

: 1351814-69-1
cyclopentyl (2S)-[(4-{[{[2,4-dihydroxy-5-(propan-2-yl)phenyl]carbonyl}(methyl)amino]methyl}benzyl)amino](phenyl)ethanoate

Guidance literature:: With hydrogen; potassium carbonate; palladium 10% on activated carbon; In ethyl acetate; at 20 ℃;

Reference yield:

: 912545-08-5
2,4-bis-benzyloxy-5-isopropenyl-benzoic acid methyl ester

: 1351814-69-1
cyclopentyl (2S)-[(4-{[{[2,4-dihydroxy-5-(propan-2-yl)phenyl]carbonyl}(methyl)amino]methyl}benzyl)amino](phenyl)ethanoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide; methanol / 20 h / 75 °C

1.2: 0.5 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h

3.1: manganese(IV) oxide / dichloromethane / 0.17 h

4.1: sodium tris(acetoxy)borohydride / 1,1-dichloroethane / 20 °C

4.2: 20 °C

5.1: potassium carbonate; hydrogen / palladium 10% on activated carbon / ethyl acetate / 20 °C

With methanol; manganese(IV) oxide; hydrogen; sodium tris(acetoxy)borohydride; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; potassium hydroxide; palladium 10% on activated carbon; In 1,1-dichloroethane; dichloromethane; ethyl acetate;

Reference yield:

: 56-91-7
p-aminomethylbenzoic acid

: 1351814-69-1
cyclopentyl (2S)-[(4-{[{[2,4-dihydroxy-5-(propan-2-yl)phenyl]carbonyl}(methyl)amino]methyl}benzyl)amino](phenyl)ethanoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydrogencarbonate / tetrahydrofuran / 48 h / 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C / Cooling with ice; Reflux

3.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h

4.1: manganese(IV) oxide / dichloromethane / 0.17 h

5.1: sodium tris(acetoxy)borohydride / 1,1-dichloroethane / 20 °C

5.2: 20 °C

6.1: potassium carbonate; hydrogen / palladium 10% on activated carbon / ethyl acetate / 20 °C

With manganese(IV) oxide; lithium aluminium tetrahydride; hydrogen; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; palladium 10% on activated carbon; In tetrahydrofuran; 1,1-dichloroethane; dichloromethane; ethyl acetate;