cyclopentyl (2S)-[(4-{[{[2,4-bis(benzyloxy)-5-(prop-1-en-2-yl)phenyl]carbonyl}(methyl)amino]methyl}benzyl)amino](phenyl)ethanoate

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Chemical Name:cyclopentyl (2S)-[(4-{[{[2,4-bis(benzyloxy)-5-(prop-1-en-2-yl)phenyl]carbonyl}(methyl)amino]methyl}benzyl)amino](phenyl)ethanoate
CAS No.:1351815-73-0
Molecular Formula:C₄₆H₄₈N₂O₅
Molecular Weight:708.898
Hs Code.:

Synonyms:cyclopentyl (2S)-[(4-{[{[2,4-bis(benzyloxy)-5-(prop-1-en-2-yl)phenyl]carbonyl}(methyl)amino]methyl}benzyl)amino](phenyl)ethanoate

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Chemical Property of cyclopentyl (2S)-[(4-{[{[2,4-bis(benzyloxy)-5-(prop-1-en-2-yl)phenyl]carbonyl}(methyl)amino]methyl}benzyl)amino](phenyl)ethanoate

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Technology Process of cyclopentyl (2S)-[(4-{[{[2,4-bis(benzyloxy)-5-(prop-1-en-2-yl)phenyl]carbonyl}(methyl)amino]methyl}benzyl)amino](phenyl)ethanoate

There total 12 articles about cyclopentyl (2S)-[(4-{[{[2,4-bis(benzyloxy)-5-(prop-1-en-2-yl)phenyl]carbonyl}(methyl)amino]methyl}benzyl)amino](phenyl)ethanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 914604-52-7
(1S)-2-(cyclopentyloxy)-2-oxo-1-phenylethanaminium 4-methylbenzenesulfonate

: 1351815-52-5
2,4-bis(benzyloxy)-N-(4-formylbenzyl)-N-methyl-5-(prop-1-en-2-yl)benzamide

: 1351815-73-0
cyclopentyl (2S)-[(4-{[{[2,4-bis(benzyloxy)-5-(prop-1-en-2-yl)phenyl]carbonyl}(methyl)amino]methyl}benzyl)amino](phenyl)ethanoate

Guidance literature:: (1S)-2-(cyclopentyloxy)-2-oxo-1-phenylethanaminium 4-methylbenzenesulfonate; 2,4-bis(benzyloxy)-N-(4-formylbenzyl)-N-methyl-5-(prop-1-en-2-yl)benzamide; With sodium tris(acetoxy)borohydride; In 1,1-dichloroethane; at 20 ℃;

With ammonium chloride; In 1,1-dichloroethane; ethyl acetate; at 20 ℃;

Reference yield:

: 912545-08-5
2,4-bis-benzyloxy-5-isopropenyl-benzoic acid methyl ester

: 1351815-73-0
cyclopentyl (2S)-[(4-{[{[2,4-bis(benzyloxy)-5-(prop-1-en-2-yl)phenyl]carbonyl}(methyl)amino]methyl}benzyl)amino](phenyl)ethanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide; methanol / 20 h / 75 °C

1.2: 0.5 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h

3.1: manganese(IV) oxide / dichloromethane / 0.17 h

4.1: sodium tris(acetoxy)borohydride / 1,1-dichloroethane / 20 °C

4.2: 20 °C

With methanol; manganese(IV) oxide; sodium tris(acetoxy)borohydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; potassium hydroxide; In 1,1-dichloroethane; dichloromethane;

Reference yield:

: 2150-47-2
methyl 2,4-dihydroxybenzoate

: 1351815-73-0
cyclopentyl (2S)-[(4-{[{[2,4-bis(benzyloxy)-5-(prop-1-en-2-yl)phenyl]carbonyl}(methyl)amino]methyl}benzyl)amino](phenyl)ethanoate

Guidance literature:: Multi-step reaction with 8 steps

1.1: dmap / 1 h / 55 °C

2.1: trifluorormethanesulfonic acid / toluene / 2.5 h / 20 °C / Cooling with ice

2.2: 18 h / 20 °C

3.1: potassium carbonate / acetonitrile / 42 h / 75 °C

4.1: potassium tert-butylate / tetrahydrofuran / 0.5 h

4.2: 0.5 h

5.1: potassium hydroxide; methanol / 20 h / 75 °C

5.2: 0.5 h / 20 °C

6.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h

7.1: manganese(IV) oxide / dichloromethane / 0.17 h

8.1: sodium tris(acetoxy)borohydride / 1,1-dichloroethane / 20 °C

8.2: 20 °C

With methanol; manganese(IV) oxide; trifluorormethanesulfonic acid; potassium tert-butylate; sodium tris(acetoxy)borohydride; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; potassium hydroxide; dmap; In tetrahydrofuran; 1,1-dichloroethane; dichloromethane; toluene; acetonitrile;