N-(4-bromobenzylidene)-bis(4-methoxy-3,5-di-tert-butylphenyl)methylamine

Base Information

Chemical Name:N-(4-bromobenzylidene)-bis(4-methoxy-3,5-di-tert-butylphenyl)methylamine
CAS No.:1072879-01-6
Molecular Formula:C₃₈H₅₂BrNO₂
Molecular Weight:634.74
Hs Code.:

Synonyms:N-(4-bromobenzylidene)-bis(4-methoxy-3,5-di-tert-butylphenyl)methylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4-bromobenzylidene)-bis(4-methoxy-3,5-di-tert-butylphenyl)methylamine

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Technology Process of N-(4-bromobenzylidene)-bis(4-methoxy-3,5-di-tert-butylphenyl)methylamine

There total 1 articles about N-(4-bromobenzylidene)-bis(4-methoxy-3,5-di-tert-butylphenyl)methylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1072879-55-0
3,3',5,5'-tetra-t-butyl-4,4'-dimethoxy benzhydrylamine

: 1122-91-4
4-bromo-benzaldehyde

: 1072879-01-6
N-(4-bromobenzylidene)-bis(4-methoxy-3,5-di-tert-butylphenyl)methylamine

Guidance literature:: 3,3',5,5'-tetra-t-butyl-4,4'-dimethoxy benzhydrylamine; With magnesium sulfate; In dichloromethane; for 0.0833333h; Inert atmosphere;

4-bromo-benzaldehyde; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ol802431v

Reference yield: 99.0%

: 623-73-4
diazoacetic acid ethyl ester

: 1072879-01-6
N-(4-bromobenzylidene)-bis(4-methoxy-3,5-di-tert-butylphenyl)methylamine

: 1072879-29-8
(2R,3R)-cis-1-(N-1-bis(4-methoxy-3,5-di-tert-butylphenyl)methyl)-2-carboxyethyl-3-(4-bromophenyl)aziridine

Guidance literature:: N-(4-bromobenzylidene)-bis(4-methoxy-3,5-di-tert-butylphenyl)methylamine; With triphenylborane; (3S)-(+)-2,2'-diphenyl-(3,3'-biphenanthrene)-4,4'-diol; In toluene; at 25 ℃; for 0.0833333h; Inert atmosphere;

diazoacetic acid ethyl ester; In toluene; at 25 ℃; for 24h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol802431v

Reference yield:

: 623-73-4
diazoacetic acid ethyl ester

: 1072879-01-6
N-(4-bromobenzylidene)-bis(4-methoxy-3,5-di-tert-butylphenyl)methylamine

: 1072879-82-3
C₄₂H₅₈BrNO₄

Guidance literature:: With C₃₈H₅₂BrNO₂*C₅₂H₃₄B₃O₇^(1-)*H⁽¹⁺⁾; In tolune-d8; at 25 ℃; for 2h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja904589k