N,N-diphenyl-4-[2-[4-(4,4,5,5-tetramethyl-1, 3,2-dioxaborolan-2-yl)phenyl]ethenyl]-benzenamine

Base Information

Chemical Name:N,N-diphenyl-4-[2-[4-(4,4,5,5-tetramethyl-1, 3,2-dioxaborolan-2-yl)phenyl]ethenyl]-benzenamine
CAS No.:1404053-06-0
Molecular Formula:C₃₂H₃₂BNO₂
Molecular Weight:473.423
Hs Code.:

Synonyms:N,N-diphenyl-4-[2-[4-(4,4,5,5-tetramethyl-1, 3,2-dioxaborolan-2-yl)phenyl]ethenyl]-benzenamine

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Chemical Property of N,N-diphenyl-4-[2-[4-(4,4,5,5-tetramethyl-1, 3,2-dioxaborolan-2-yl)phenyl]ethenyl]-benzenamine

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Technology Process of N,N-diphenyl-4-[2-[4-(4,4,5,5-tetramethyl-1, 3,2-dioxaborolan-2-yl)phenyl]ethenyl]-benzenamine

There total 2 articles about N,N-diphenyl-4-[2-[4-(4,4,5,5-tetramethyl-1, 3,2-dioxaborolan-2-yl)phenyl]ethenyl]-benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 219987-44-7
N-{4-[2-(4-bromophenyl)vinyl]phenyl}-diphenylamine

: 73183-34-3
bis(pinacol)diborane

: 1404053-06-0
N,N-diphenyl-4-[2-[4-(4,4,5,5-tetramethyl-1, 3,2-dioxaborolan-2-yl)phenyl]ethenyl]-benzenamine

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; potassium acetate; triphenylphosphine; In toluene; at 120 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c2cc35754b

Reference yield:

: 2039-82-9
1-bromo-4-ethenyl-benzene

: 38257-52-2
4-(N,N-diphenylamino)iodobenzene

: 1404053-06-0
N,N-diphenyl-4-[2-[4-(4,4,5,5-tetramethyl-1, 3,2-dioxaborolan-2-yl)phenyl]ethenyl]-benzenamine

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; tetrabutylammomium bromide / N,N-dimethyl-formamide / 36 h / 60 °C / Inert atmosphere; Alkaline conditions

2: bis-triphenylphosphine-palladium(II) chloride; potassium acetate; triphenylphosphine / toluene / 24 h / 120 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; tetrabutylammomium bromide; potassium acetate; palladium diacetate; triphenylphosphine; In N,N-dimethyl-formamide; toluene; 1: |Heck Reaction / 2: |Miyaura Borylation Reaction;
DOI:10.1039/c2cc35754b

Reference yield: 88.0%

: 1192352-10-5
4,7-bis(5-bromothiophen-2-yl)-5,6-bis(tetradecyloxy)benzo[c][1,2,5]thiadiazole

: 1404053-06-0
N,N-diphenyl-4-[2-[4-(4,4,5,5-tetramethyl-1, 3,2-dioxaborolan-2-yl)phenyl]ethenyl]-benzenamine

: 1404053-08-2
4,7-bis{5-{4-{2-[4-(N,N-diphenylamino)phenyl]-1-ethenyl}phenyl}-2-thienyl}-5,6,-bis(otcyloxy)-2,1,3-benzothiadiazole

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; water; toluene; at 110 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c2cc35754b