2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)methyl phosphate-4,5-bis(dibenzyl) phosphate

Base Information

Chemical Name:2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)methyl phosphate-4,5-bis(dibenzyl) phosphate
CAS No.:252868-85-2
Molecular Formula:C₇₆H₁₁₅O₁₈P₃
Molecular Weight:1409.66
Hs Code.:

Synonyms:2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)methyl phosphate-4,5-bis(dibenzyl) phosphate

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Chemical Property of 2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)methyl phosphate-4,5-bis(dibenzyl) phosphate

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Technology Process of 2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)methyl phosphate-4,5-bis(dibenzyl) phosphate

There total 3 articles about 2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)methyl phosphate-4,5-bis(dibenzyl) phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 108549-23-1
Dibenzyl N,N-diisopropylphosphoramidite

: 252868-80-7
2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)methyl phosphate

: 252868-85-2
2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)methyl phosphate-4,5-bis(dibenzyl) phosphate

Guidance literature:: Dibenzyl N,N-diisopropylphosphoramidite; 2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)methyl phosphate; With 1H-tetrazole; In dichloromethane; at 20 ℃; for 6h;

With tert.-butylhydroperoxide; In dichloromethane;
DOI:10.1016/S0040-4020(99)00793-0

Reference yield:

: 496808-59-4
Hexadecanoic acid (R)-2-(diisopropylamino-methoxy-phosphanyloxy)-1-hexadecanoyloxymethyl-ethyl ester

: 252868-85-2
2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)methyl phosphate-4,5-bis(dibenzyl) phosphate

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrazole / CH₂Cl₂ / 6 h / 20 °C

1.2: 40 percent / t-BuOOH / CH₂Cl₂

2.1: H₂ / Pd/C / ethanol / 4 h / 20 °C / 3878.61 Torr

3.1: tetrazole / CH₂Cl₂ / 6 h / 20 °C

3.2: 60 percent / t-BuOOH / CH₂Cl₂

With 1H-tetrazole; hydrogen; palladium on activated charcoal; In ethanol; dichloromethane; 1.1: Substitution / 1.2: Oxidation / 2.1: Hydrogenolysis / 3.1: Substitution / 3.2: Oxidation;
DOI:10.1016/S0040-4020(99)00793-0

Reference yield:

: 252868-77-2
4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)methyl phosphate

: 252868-85-2
2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)methyl phosphate-4,5-bis(dibenzyl) phosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: H₂ / Pd/C / ethanol / 4 h / 20 °C / 3878.61 Torr

2.1: tetrazole / CH₂Cl₂ / 6 h / 20 °C

2.2: 60 percent / t-BuOOH / CH₂Cl₂

With 1H-tetrazole; hydrogen; palladium on activated charcoal; In ethanol; dichloromethane; 1.1: Hydrogenolysis / 2.1: Substitution / 2.2: Oxidation;
DOI:10.1016/S0040-4020(99)00793-0