4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)methyl phosphate

Base Information

Chemical Name:4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)methyl phosphate
CAS No.:252868-77-2
Molecular Formula:C₅₅H₉₅O₁₂P
Molecular Weight:979.326
Hs Code.:

Synonyms:4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)methyl phosphate

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Chemical Property of 4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)methyl phosphate

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Technology Process of 4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)methyl phosphate

There total 1 articles about 4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)methyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 496808-59-4
Hexadecanoic acid (R)-2-(diisopropylamino-methoxy-phosphanyloxy)-1-hexadecanoyloxymethyl-ethyl ester

: 156593-40-7
D-4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-myo-inositol

: 4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1,5-cyclic(methyl)phosphate

: 252868-77-2
4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)methyl phosphate

Guidance literature:: Hexadecanoic acid (R)-2-(diisopropylamino-methoxy-phosphanyloxy)-1-hexadecanoyloxymethyl-ethyl ester; D-4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-myo-inositol; With 1H-tetrazole; In dichloromethane; at 20 ℃; for 6h;

With tert.-butylhydroperoxide; In dichloromethane;
DOI:10.1016/S0040-4020(99)00793-0

Reference yield:

: 252868-77-2
4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)methyl phosphate

: 6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)methyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / ethanol / 4 h / 20 °C / 3878.61 Torr

2: 90 percent / HCl / methanol / 3 h / 20 °C

With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; ethanol; 1: Hydrogenolysis / 2: Ring cleavage;
DOI:10.1016/S0040-4020(99)00793-0

Reference yield:

: 252868-77-2
4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)methyl phosphate

: 252868-85-2
2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)methyl phosphate-4,5-bis(dibenzyl) phosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: H₂ / Pd/C / ethanol / 4 h / 20 °C / 3878.61 Torr

2.1: tetrazole / CH₂Cl₂ / 6 h / 20 °C

2.2: 60 percent / t-BuOOH / CH₂Cl₂

With 1H-tetrazole; hydrogen; palladium on activated charcoal; In ethanol; dichloromethane; 1.1: Hydrogenolysis / 2.1: Substitution / 2.2: Oxidation;
DOI:10.1016/S0040-4020(99)00793-0