Diphenyl-[9-(3`-O-tert-butyldiphenylsilyl-2`,5`,6`-trideoxy-β-D-erythro-hexofuranosyl)-6-N-benzoyladenin-6`-yl]phosphonate

Base Information

Chemical Name:Diphenyl-[9-(3`-O-tert-butyldiphenylsilyl-2`,5`,6`-trideoxy-β-D-erythro-hexofuranosyl)-6-N-benzoyladenin-6`-yl]phosphonate
CAS No.:250650-18-1
Molecular Formula:C₄₆H₄₆N₅O₆PSi
Molecular Weight:823.96
Hs Code.:

Synonyms:Diphenyl-[9-(3`-O-tert-butyldiphenylsilyl-2`,5`,6`-trideoxy-β-D-erythro-hexofuranosyl)-6-N-benzoyladenin-6`-yl]phosphonate

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Chemical Property of Diphenyl-[9-(3`-O-tert-butyldiphenylsilyl-2`,5`,6`-trideoxy-β-D-erythro-hexofuranosyl)-6-N-benzoyladenin-6`-yl]phosphonate

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Technology Process of Diphenyl-[9-(3`-O-tert-butyldiphenylsilyl-2`,5`,6`-trideoxy-β-D-erythro-hexofuranosyl)-6-N-benzoyladenin-6`-yl]phosphonate

There total 4 articles about Diphenyl-[9-(3`-O-tert-butyldiphenylsilyl-2`,5`,6`-trideoxy-β-D-erythro-hexofuranosyl)-6-N-benzoyladenin-6`-yl]phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 250650-03-4
Diphenyl-[9-(3`-O-tert-butyldiphenylsilyl-2`,5`,6`-trideoxy-β-D-erythro-hex-5-enofuranosyl)-6-N-benzoyladenin-6`-yl]phosphonate

: 250650-18-1
Diphenyl-[9-(3`-O-tert-butyldiphenylsilyl-2`,5`,6`-trideoxy-β-D-erythro-hexofuranosyl)-6-N-benzoyladenin-6`-yl]phosphonate

Guidance literature:: With potassium diazodicarboxylate; In pyridine; acetic acid; for 4h;
DOI:10.1039/a906066i

Reference yield:

: 22400-41-5
diphenyl [(triphenylphosphoranylidene)methyl]phosphonate

: 250650-18-1
Diphenyl-[9-(3`-O-tert-butyldiphenylsilyl-2`,5`,6`-trideoxy-β-D-erythro-hexofuranosyl)-6-N-benzoyladenin-6`-yl]phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylsulfoxide

2: 88 percent / potassium azodicarboxylate / pyridine; acetic acid / 4 h

With potassium diazodicarboxylate; In pyridine; acetic acid; dimethyl sulfoxide; 1: Condensation / 2: Reduction;
DOI:10.1039/a906066i

Reference yield:

: 111570-92-4
N⁶-benzoyl-3'-O-(tert-butyldiphenylsilyl)-2'-deoxyadenosine

: 250650-18-1
Diphenyl-[9-(3`-O-tert-butyldiphenylsilyl-2`,5`,6`-trideoxy-β-D-erythro-hexofuranosyl)-6-N-benzoyladenin-6`-yl]phosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 1,3-dicyclohexylcarbodiimide; pyridine; CF₃COOH / dimethylsulfoxide / 7 h

2: dimethylsulfoxide

3: 88 percent / potassium azodicarboxylate / pyridine; acetic acid / 4 h

With pyridine; potassium diazodicarboxylate; dicyclohexyl-carbodiimide; trifluoroacetic acid; In pyridine; acetic acid; dimethyl sulfoxide; 1: Oxidation / 2: Condensation / 3: Reduction;
DOI:10.1039/a906066i