benzhydryl-(8-tert-butyl-1,2-dioxaspiro[4.5]dec-3-ylmethyl)-dimethylsilane

Base Information

Chemical Name:benzhydryl-(8-tert-butyl-1,2-dioxaspiro[4.5]dec-3-ylmethyl)-dimethylsilane
CAS No.:869298-33-9
Molecular Formula:C₂₈H₄₀O₂Si
Molecular Weight:436.71
Hs Code.:

Synonyms:benzhydryl-(8-tert-butyl-1,2-dioxaspiro[4.5]dec-3-ylmethyl)-dimethylsilane

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Chemical Property of benzhydryl-(8-tert-butyl-1,2-dioxaspiro[4.5]dec-3-ylmethyl)-dimethylsilane

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Technology Process of benzhydryl-(8-tert-butyl-1,2-dioxaspiro[4.5]dec-3-ylmethyl)-dimethylsilane

There total 3 articles about benzhydryl-(8-tert-butyl-1,2-dioxaspiro[4.5]dec-3-ylmethyl)-dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 960121-25-9
1,1-di(triethylsilyldioxy)-4-tert-butylcyclohexane

: 274676-28-7
allylbenzhydryldimethylsilane

: 869298-33-9
benzhydryl-(8-tert-butyl-1,2-dioxaspiro[4.5]dec-3-ylmethyl)-dimethylsilane

Guidance literature:: With tin(IV) chloride; In dichloromethane; at -78 - 25 ℃; for 22h;
DOI:10.1021/ol051703u

Reference yield:

: 98-53-3
4-tercbutyl-cyclohexanone

: 869298-33-9
benzhydryl-(8-tert-butyl-1,2-dioxaspiro[4.5]dec-3-ylmethyl)-dimethylsilane

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / 3 Angstroem molecular sieves; formic acid; aq. H₂O₂ / CH₂Cl₂ / 0.05 h / 25 °C

2: 73 percent / Et₃N / dimethylformamide

3: 72 percent / SnCl₄ / CH₂Cl₂ / 22 h / -78 - 25 °C

With formic acid; 3 A molecular sieve; dihydrogen peroxide; tin(IV) chloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol051703u

Reference yield:

: 229323-96-0
1,1-dihydroperoxy-(4-tert-butyl)cyclohexane

: 869298-33-9
benzhydryl-(8-tert-butyl-1,2-dioxaspiro[4.5]dec-3-ylmethyl)-dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / Et₃N / dimethylformamide

2: 72 percent / SnCl₄ / CH₂Cl₂ / 22 h / -78 - 25 °C

With tin(IV) chloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol051703u