2-chloro-4-nitrophenyl phosphorodichloridate

Base Information

Chemical Name:2-chloro-4-nitrophenyl phosphorodichloridate
CAS No.:20056-43-3
Molecular Formula:C₆H₃Cl₃NO₄P
Molecular Weight:290.427
Hs Code.:

Synonyms:2-chloro-4-nitrophenyl phosphorodichloridate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-chloro-4-nitrophenyl phosphorodichloridate

Chemical Property:

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Technology Process of 2-chloro-4-nitrophenyl phosphorodichloridate

There total 2 articles about 2-chloro-4-nitrophenyl phosphorodichloridate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 619-08-9
2-chloro-4-nitrophenol

: 20056-43-3
2-chloro-4-nitrophenyl phosphorodichloridate

Guidance literature:: With sodium chloride; trichlorophosphate; for 6h; Heating;
DOI:10.1039/P29800000373

Reference yield:

: 20056-43-3
2-chloro-4-nitrophenyl phosphorodichloridate

Guidance literature:: Phenol, POCl3;

Reference yield:

: 20056-43-3
2-chloro-4-nitrophenyl phosphorodichloridate

: 115142-08-0
Phosphoric acid 2-chloro-4-nitro-phenyl ester (2R,3S,4R,5R)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-4-hydroxy-2-hydroxymethyl-tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1,2,4-triazole, triethylamine, pyridine / acetonitrile / 2 h / Ambient temperature

2: Amberlyst 15 ion-exchange resin / H₂O / 0.5 h / Ambient temperature

With pyridine; 1,2,4-Triazole; Amberlyst 15 ion-exchange resin; triethylamine; In water; acetonitrile;
DOI:10.1021/ja00223a031