Technology Process of C17H25BFNO6
There total 5 articles about C17H25BFNO6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate;
In
1,4-dioxane;
for 16h;
Reflux;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C / Reflux; Inert atmosphere
1.2: 16 h / 20 °C
2.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 48 h / 20 °C
3.1: tetra-n-butylammonium dihydrogen trifluoride; potassium hydrogen bifluoride / 6 h / 120 °C
4.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate / 1,4-dioxane / 16 h / Reflux; Inert atmosphere
With
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium hydrogen bifluoride; potassium acetate; sodium hydride; tetra-n-butylammonium dihydrogen trifluoride; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; 1,4-dioxane; chloroform; mineral oil;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C / Reflux; Inert atmosphere
1.2: 16 h / 20 °C
2.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 48 h / 20 °C
3.1: tetra-n-butylammonium dihydrogen trifluoride; potassium hydrogen bifluoride / 6 h / 120 °C
4.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate / 1,4-dioxane / 16 h / Reflux; Inert atmosphere
With
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium hydrogen bifluoride; potassium acetate; sodium hydride; tetra-n-butylammonium dihydrogen trifluoride; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; 1,4-dioxane; chloroform; mineral oil;