3-((((2-Chlorophenyl)azo)phenylmethylene)amino)-2-methyl-4(3H)-quinazolinone

Base Information

Chemical Name:3-((((2-Chlorophenyl)azo)phenylmethylene)amino)-2-methyl-4(3H)-quinazolinone
CAS No.:110621-87-9
Molecular Formula:C₂₂H₁₆ClN₅O
Molecular Weight:401.855
Hs Code.:
NSC Number:622350
ChEMBL ID:CHEMBL1989850

Synonyms:BRN 5148374;3-((((2-Chlorophenyl)azo)phenylmethylene)amino)-2-methyl-4(3H)-quinazolinone;4(3H)-Quinazolinone, 3-((((2-chlorophenyl)azo)phenylmethylene)amino)-2-methyl-;alpha-(o-Chlorophenylazo)-N-2-methyl-4(3H)-oxo-3-quinazolinylbenzylidenimine;110621-87-9;NSC622350;CHEMBL1989850;NSC-622350;LS-140547

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-((((2-Chlorophenyl)azo)phenylmethylene)amino)-2-methyl-4(3H)-quinazolinone

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:570.531°C at 760 mmHg
Flash Point:298.847°C
Density:1.305g/cm³
XLogP3:5.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:401.1043378
Heavy Atom Count:29
Complexity:685

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=NC2=CC=CC=C2C(=O)N1N=C(C3=CC=CC=C3)N=NC4=CC=CC=C4Cl
Isomeric SMILES:CC1=NC2=CC=CC=C2C(=O)N1/N=C(/C3=CC=CC=C3)\N=NC4=CC=CC=C4Cl

Technology Process of 3-((((2-Chlorophenyl)azo)phenylmethylene)amino)-2-methyl-4(3H)-quinazolinone

There total 3 articles about 3-((((2-Chlorophenyl)azo)phenylmethylene)amino)-2-methyl-4(3H)-quinazolinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1898-06-2
3-amino-2-methyl-4-oxoquinazoline

: 110621-87-9
C₂₂H₁₆ClN₅O

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / gl. acetic acid / ethanol / 5 h / Heating

2: 1) aq. NaNO₂, gl. acetic acid, HCl / 1) 0-5 deg C, 2) pyridine, r.t., overnight

With hydrogenchloride; acetic acid; sodium nitrite; In ethanol;

Reference yield:

: 100-52-7
benzaldehyde

: 110621-87-9
C₂₂H₁₆ClN₅O

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / gl. acetic acid / ethanol / 5 h / Heating

2: 1) aq. NaNO₂, gl. acetic acid, HCl / 1) 0-5 deg C, 2) pyridine, r.t., overnight

With hydrogenchloride; acetic acid; sodium nitrite; In ethanol;

Reference yield:

: 56158-74-8
2-methyl-3-(phenylmethylene)-amino-4(3H)quinazolinone

: 95-51-2
o-chloroaniline

: 110621-87-9
C₂₂H₁₆ClN₅O

Guidance literature:: With hydrogenchloride; acetic acid; sodium nitrite; Yield given. Multistep reaction; 1) 0-5 deg C, 2) pyridine, r.t., overnight;