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Technology Process of (CH3CH2CH2N(CH2CH2P(C6H5)2)2)RuCl(CO)(C(CH2C6H5)NHC6H5)(1+)*PF6(1-)=[(C31H35NP2)RuCl(CO)(C(CH2C6H5)NHC6H5)]PF6

(CH3CH2CH2N(CH2CH2P(C6H5)2)2)RuCl(CO)(C(CH2C6H5)NHC6H5)(1+)*PF6(1-)=[(C31H35NP2)RuCl(CO)(C(CH2C6H5)NHC6H5)]PF6

Base Information
  • Chemical Name:(CH3CH2CH2N(CH2CH2P(C6H5)2)2)RuCl(CO)(C(CH2C6H5)NHC6H5)(1+)*PF6(1-)=[(C31H35NP2)RuCl(CO)(C(CH2C6H5)NHC6H5)]PF6
  • CAS No.:206365-14-2
  • Molecular Formula:C46H48ClN2OP2Ru*F6P
  • Molecular Weight:988.335
  • Hs Code.:
(CH<sub>3</sub>CH<sub>2</sub>CH<sub>2</sub>N(CH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2)RuCl(CO)(C(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)NHC<sub>6</sub>H<sub>5</sub>)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=[(C<sub>31</sub>H<sub>35</sub>NP<sub>2</sub>)RuCl(CO)(C(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)NHC<sub>6</sub>H<sub>5</sub>)]PF<sub>6</sub>

Synonyms:(CH3CH2CH2N(CH2CH2P(C6H5)2)2)RuCl(CO)(C(CH2C6H5)NHC6H5)(1+)*PF6(1-)=[(C31H35NP2)RuCl(CO)(C(CH2C6H5)NHC6H5)]PF6

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Chemical Property of (CH3CH2CH2N(CH2CH2P(C6H5)2)2)RuCl(CO)(C(CH2C6H5)NHC6H5)(1+)*PF6(1-)=[(C31H35NP2)RuCl(CO)(C(CH2C6H5)NHC6H5)]PF6
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Technology Process of (CH3CH2CH2N(CH2CH2P(C6H5)2)2)RuCl(CO)(C(CH2C6H5)NHC6H5)(1+)*PF6(1-)=[(C31H35NP2)RuCl(CO)(C(CH2C6H5)NHC6H5)]PF6

There total 2 articles about (CH3CH2CH2N(CH2CH2P(C6H5)2)2)RuCl(CO)(C(CH2C6H5)NHC6H5)(1+)*PF6(1-)=[(C31H35NP2)RuCl(CO)(C(CH2C6H5)NHC6H5)]PF6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

fac,cis-[(CH<sub>3</sub>CH<sub>2</sub>CH<sub>2</sub>N(CH<sub>2</sub>CH<sub>2</sub>PPh<sub>2</sub>)2)RuCl<sub>2</sub>(=C(NHPh)CH<sub>2</sub>Ph)]

fac,cis-[(CH3CH2CH2N(CH2CH2PPh2)2)RuCl2(=C(NHPh)CH2Ph)]

carbon monoxide
201230-82-2

carbon monoxide

(CH<sub>3</sub>CH<sub>2</sub>CH<sub>2</sub>N(CH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2)RuCl(CO)(C(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)NHC<sub>6</sub>H<sub>5</sub>)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=[(C<sub>31</sub>H<sub>35</sub>NP<sub>2</sub>)RuCl(CO)(C(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)NHC<sub>6</sub>H<sub>5</sub>)]PF<sub>6</sub>
206365-14-2

(CH3CH2CH2N(CH2CH2P(C6H5)2)2)RuCl(CO)(C(CH2C6H5)NHC6H5)(1+)*PF6(1-)=[(C31H35NP2)RuCl(CO)(C(CH2C6H5)NHC6H5)]PF6

Guidance literature:
With thallium(I) hexafluorophosphate; In not given; in CO-stream;
DOI:10.1016/s0020-1693(97)05877-5

Reference yield: 80.0%

mer-[(CH<sub>3</sub>CH<sub>2</sub>CH<sub>2</sub>N(CH<sub>2</sub>CH<sub>2</sub>PPh<sub>2</sub>)2)RuCl(C=C(H)Ph)(C(N(H)Ph)(CH<sub>2</sub>Ph))]PF<sub>6</sub>
206365-12-0

mer-[(CH3CH2CH2N(CH2CH2PPh2)2)RuCl(C=C(H)Ph)(C(N(H)Ph)(CH2Ph))]PF6

carbon monoxide
201230-82-2

carbon monoxide

(CH<sub>3</sub>CH<sub>2</sub>CH<sub>2</sub>N(CH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2)RuCl(CO)(C(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)NHC<sub>6</sub>H<sub>5</sub>)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=[(C<sub>31</sub>H<sub>35</sub>NP<sub>2</sub>)RuCl(CO)(C(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)NHC<sub>6</sub>H<sub>5</sub>)]PF<sub>6</sub>
206365-14-2

(CH3CH2CH2N(CH2CH2P(C6H5)2)2)RuCl(CO)(C(CH2C6H5)NHC6H5)(1+)*PF6(1-)=[(C31H35NP2)RuCl(CO)(C(CH2C6H5)NHC6H5)]PF6

Guidance literature:
In tetrahydrofuran; byproducts: PhC2H; refluxing in CO-atmosphere for 30 min; cooling to room temp., crystn. on hexane addn.; elem. anal.;
DOI:10.1016/s0020-1693(97)05877-5
upstream raw materials:

carbon monoxide

mer-[(CH3CH2CH2N(CH2CH2PPh2)2)RuCl(C=C(H)Ph)(C(N(H)Ph)(CH2Ph))]PF6

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