N-(6-carboxyhexyl)-4-phenoxy-1,8-naphthalimide methyl ester

Base Information

Chemical Name:N-(6-carboxyhexyl)-4-phenoxy-1,8-naphthalimide methyl ester
CAS No.:1357477-70-3
Molecular Formula:C₂₅H₂₃NO₅
Molecular Weight:417.461
Hs Code.:

Synonyms:N-(6-carboxyhexyl)-4-phenoxy-1,8-naphthalimide methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(6-carboxyhexyl)-4-phenoxy-1,8-naphthalimide methyl ester

Chemical Property:

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Technology Process of N-(6-carboxyhexyl)-4-phenoxy-1,8-naphthalimide methyl ester

There total 3 articles about N-(6-carboxyhexyl)-4-phenoxy-1,8-naphthalimide methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1357477-68-9
methyl 6-(6-bromo-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)hexanoate

: 108-95-2,27073-41-2
phenol

: 1357477-70-3
N-(6-carboxyhexyl)-4-phenoxy-1,8-naphthalimide methyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 8h; Inert atmosphere;
DOI:10.1039/c2jm13826c

Reference yield:

methyl 6-aminohexanoate hydrochloride: 2780-89-4
methyl 6-aminohexanoate hydrochloride

: 1357477-70-3
N-(6-carboxyhexyl)-4-phenoxy-1,8-naphthalimide methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 12 h / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 8 h / 100 °C / Inert atmosphere

With potassium carbonate; In N,N-dimethyl-formamide; toluene;
DOI:10.1039/c2jm13826c

Reference yield:

: 81-86-7
4-bromo-1,8-naphthalenedicarboxylic anhydride

: 1357477-70-3
N-(6-carboxyhexyl)-4-phenoxy-1,8-naphthalimide methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 12 h / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 8 h / 100 °C / Inert atmosphere

With potassium carbonate; In N,N-dimethyl-formamide; toluene;
DOI:10.1039/c2jm13826c