[3-({Bis-[2-(5-ethyl-pyridin-2-yl)-ethyl]-amino}-methyl)-5-nitro-benzyl]-bis-[2-(5-ethyl-pyridin-2-yl)-ethyl]-amine

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Chemical Name:[3-({Bis-[2-(5-ethyl-pyridin-2-yl)-ethyl]-amino}-methyl)-5-nitro-benzyl]-bis-[2-(5-ethyl-pyridin-2-yl)-ethyl]-amine
CAS No.:154742-99-1
Molecular Formula:C₄₄H₅₅N₇O₂
Molecular Weight:713.966
Hs Code.:

Synonyms:[3-({Bis-[2-(5-ethyl-pyridin-2-yl)-ethyl]-amino}-methyl)-5-nitro-benzyl]-bis-[2-(5-ethyl-pyridin-2-yl)-ethyl]-amine

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Chemical Property of [3-({Bis-[2-(5-ethyl-pyridin-2-yl)-ethyl]-amino}-methyl)-5-nitro-benzyl]-bis-[2-(5-ethyl-pyridin-2-yl)-ethyl]-amine

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Technology Process of [3-({Bis-[2-(5-ethyl-pyridin-2-yl)-ethyl]-amino}-methyl)-5-nitro-benzyl]-bis-[2-(5-ethyl-pyridin-2-yl)-ethyl]-amine

There total 5 articles about [3-({Bis-[2-(5-ethyl-pyridin-2-yl)-ethyl]-amino}-methyl)-5-nitro-benzyl]-bis-[2-(5-ethyl-pyridin-2-yl)-ethyl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 51760-20-4
1,3-bis-bromomethyl-5-nitro-benzene

: 154743-00-7
bis<2-(2-(5-ethylpyridyl)ethyl)>amine

: 154742-99-1
[3-({Bis-[2-(5-ethyl-pyridin-2-yl)-ethyl]-amino}-methyl)-5-nitro-benzyl]-bis-[2-(5-ethyl-pyridin-2-yl)-ethyl]-amine

Guidance literature:: With TEA; In ethyl acetate; at 0 - 20 ℃; for 120h;
DOI:10.1021/ja00083a018

Reference yield:

: 5408-74-2
5-ethyl-2-vinyl-pyridine

: 154742-99-1
[3-({Bis-[2-(5-ethyl-pyridin-2-yl)-ethyl]-amino}-methyl)-5-nitro-benzyl]-bis-[2-(5-ethyl-pyridin-2-yl)-ethyl]-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 16.5 percent / aq. NH₄Cl / methanol / 48 h / Heating

2: 34 percent / TEA / ethyl acetate / 120 h / 0 - 20 °C

With TEA; ammonium chloride; In methanol; ethyl acetate;
DOI:10.1021/ja00083a018

Reference yield:

: 104-90-5
5-ethyl-2-methyl-pyridine

: 154742-99-1
[3-({Bis-[2-(5-ethyl-pyridin-2-yl)-ethyl]-amino}-methyl)-5-nitro-benzyl]-bis-[2-(5-ethyl-pyridin-2-yl)-ethyl]-amine

Guidance literature:: Multi-step reaction with 4 steps

1: formic acid, tert-butylcatechol / ethanol / 120 h / Heating

2: KOH / Heating

3: 16.5 percent / aq. NH₄Cl / methanol / 48 h / Heating

4: 34 percent / TEA / ethyl acetate / 120 h / 0 - 20 °C

With potassium hydroxide; formic acid; 3-tert-butylbenzene-1,2-diol; TEA; ammonium chloride; In methanol; ethanol; ethyl acetate;
DOI:10.1021/ja00083a018