benzyl meta-chlorophenyldiazoacetate

Base Information

• Chemical Name: benzyl meta-chlorophenyldiazoacetate
• CAS No.: 1432320-55-2
• Molecular Formula: C₁₅H₁₁ClN₂O₂
• Molecular Weight: 286.718

Synonyms:benzyl meta-chlorophenyldiazoacetate

Chemical Property of benzyl meta-chlorophenyldiazoacetate

Chemical Property:

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Technology Process of benzyl meta-chlorophenyldiazoacetate

There total 1 articles about benzyl meta-chlorophenyldiazoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C15H13ClO2 → benzyl meta-chlorophenyldiazoacetate (1432320-55-2)

Guidance literature:

With 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 0 - 25 ℃; for 12h; Inert atmosphere;

DOI:10.1039/c9ob01903k

Reference yield: 78.0%

benzyl meta-chlorophenyldiazoacetate (1432320-55-2) + malonic acid dimethyl ester (108-59-8) → C20H19ClO6

Guidance literature:

With copper(l) cyanide; sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate; tricyclohexylphosphine; In chloroform; at 60 ℃; for 2h;

DOI:10.1002/cctc.202000684

Reference yield:

benzyl meta-chlorophenyldiazoacetate (1432320-55-2) → C15H11ClO2 + C15H11ClO2

Guidance literature:

With C₈₇H₈₅IrN₄O; In dichloromethane; at 25 ℃; for 0.166667h; Overall yield = 75 %; Overall yield = 80 %Spectr.; enantioselective reaction; Inert atmosphere;

DOI:10.1021/cs4001656

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