N-(3-bromo-2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)-N'-(4-methylphenylsulfonyl)benzenecarboximidamide

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Chemical Name:N-(3-bromo-2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)-N'-(4-methylphenylsulfonyl)benzenecarboximidamide
CAS No.:1332847-76-3
Molecular Formula:C₂₂H₁₉BrN₂O₃S
Molecular Weight:471.374
Hs Code.:

Synonyms:N-(3-bromo-2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)-N'-(4-methylphenylsulfonyl)benzenecarboximidamide

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Chemical Property of N-(3-bromo-2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)-N'-(4-methylphenylsulfonyl)benzenecarboximidamide

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Technology Process of N-(3-bromo-2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)-N'-(4-methylphenylsulfonyl)benzenecarboximidamide

There total 4 articles about N-(3-bromo-2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)-N'-(4-methylphenylsulfonyl)benzenecarboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1332847-63-8
N-(3-bromo-4-hydroxy-2,5-dimethylphenyl)-N'-(4-phenylphenylsulfonyl)benzenecarboximidamide

: 1332847-76-3
N-(3-bromo-2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)-N'-(4-methylphenylsulfonyl)benzenecarboximidamide

Guidance literature:: With lead(IV) tetraacetate; In acetic acid; at 20 ℃;
DOI:10.1134/S1070428011070116

Reference yield:

: 461672-30-0
N-(4-hydroxy-2,5-dimethylphenyl)-N'-(4-methylphenylsulfonyl)benzimidamide

: 1332847-76-3
N-(3-bromo-2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)-N'-(4-methylphenylsulfonyl)benzenecarboximidamide

Guidance literature:: Multi-step reaction with 3 steps

1: lead(IV) tetraacetate / acetic acid

2: hydrogen bromide / water; acetic acid / 50 - 60 °C

3: lead(IV) tetraacetate / acetic acid / 20 °C

With hydrogen bromide; lead(IV) tetraacetate; In water; acetic acid;
DOI:10.1134/S1070428011070116

Reference yield:

: 452089-45-1
N-(2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)-N'-(4-methylphenylsulfonyl)benzenecarboximidamide

: 1332847-76-3
N-(3-bromo-2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)-N'-(4-methylphenylsulfonyl)benzenecarboximidamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen bromide / water; acetic acid / 50 - 60 °C

2: lead(IV) tetraacetate / acetic acid / 20 °C

With hydrogen bromide; lead(IV) tetraacetate; In water; acetic acid;
DOI:10.1134/S1070428011070116