3-deoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-1,2-O-(1-methylethylidene)-α-D-xylofuranose

Base Information

Chemical Name:3-deoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-1,2-O-(1-methylethylidene)-α-D-xylofuranose
CAS No.:106799-13-7
Molecular Formula:C₂₄H₃₂O₄Si
Molecular Weight:412.601
Hs Code.:

Synonyms:3-deoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-1,2-O-(1-methylethylidene)-α-D-xylofuranose

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Chemical Property of 3-deoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-1,2-O-(1-methylethylidene)-α-D-xylofuranose

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Technology Process of 3-deoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-1,2-O-(1-methylethylidene)-α-D-xylofuranose

There total 9 articles about 3-deoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-1,2-O-(1-methylethylidene)-α-D-xylofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 114861-17-5
tert-Butyl-((3aR,5R,6R,6aS)-6-iodo-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-ylmethoxy)-diphenyl-silane

: 106799-13-7
3-deoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-1,2-O-(1-methylethylidene)-α-D-xylofuranose

Guidance literature:: With lithium triethylborohydride; In tetrahydrofuran; for 12h; Heating;
DOI:10.1021/ja00222a028

Reference yield: 77.0%

: 114861-15-3
5-O-<(1,1-dimethylethyl)diphenylsilyl>-1,2-O-(1-methylethylidene)-α-D-xylofuranose 3-(O-phenylthiocarbonate)

: 106799-13-7
3-deoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-1,2-O-(1-methylethylidene)-α-D-xylofuranose

Guidance literature:: With tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile); In toluene; at 80 ℃; for 1h;
DOI:10.1021/ja00241a062

Reference yield: 76.0%

: 5-O-tert-Butyl(diphenyl)silyl-1,2-O-isopropylidene-3-thiocarbonylimidazolo-D-xylofuranose

: 106799-13-7
3-deoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-1,2-O-(1-methylethylidene)-α-D-xylofuranose

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 116 ℃; for 3h; Inert atmosphere;
DOI:10.1021/acs.joc.9b00338