2,5-Cyclohexadien-1-one,4-[bis(4-methylphenyl)methylene]-2,6-bis(1,1-dimethylethyl)-

Base Information

Chemical Name:2,5-Cyclohexadien-1-one,4-[bis(4-methylphenyl)methylene]-2,6-bis(1,1-dimethylethyl)-
CAS No.:13135-02-9
Molecular Formula:C29H34 O
Molecular Weight:398.588
Hs Code.:

Synonyms:2,5-Cyclohexadien-1-one,2,6-di-tert-butyl-4-(di-p-tolylmethylene)- (8CI); 3,5-Di-tert-butyl-4',4''-dimethylfuchsone;Fuchsone, 3,5-bis(1,1-dimethylethyl)-4',4''-dimethyl-

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Chemical Property of 2,5-Cyclohexadien-1-one,4-[bis(4-methylphenyl)methylene]-2,6-bis(1,1-dimethylethyl)-

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 2,5-Cyclohexadien-1-one,4-[bis(4-methylphenyl)methylene]-2,6-bis(1,1-dimethylethyl)-

There total 6 articles about 2,5-Cyclohexadien-1-one,4-[bis(4-methylphenyl)methylene]-2,6-bis(1,1-dimethylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 70039-22-4
4-(4-methylphenyl)methylene-2,6-di-tert-butyl-2,5-cyclohexanedien-1-one

: 459-44-9
4-methylbenzenediazonium tetrafluoroborate

: 13135-02-9
4-(α,α-di-p-tolylmethylene)-2,6-di-t-butyl-1,4-benzoquinone

Guidance literature:: With ruthenium(III) chloride trihydrate; potassium carbonate; In acetonitrile; at 50 ℃; for 6h; regioselective reaction; Inert atmosphere; Schlenk technique; Sealed tube; Green chemistry;
DOI:10.1021/acs.joc.0c00621

Reference yield:

: 611-97-2
bis(p-methylphenyl)-methanone

: 13135-02-9
4-(α,α-di-p-tolylmethylene)-2,6-di-t-butyl-1,4-benzoquinone

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent

2: acid

With acid; 1: Addition / 2: Dehydration;
DOI:10.1246/cl.1999.571