5'-O-(tert-butyldimethylsilyl)-N⁶-(4-methoxytrityl)-2'-C-methyladenosine

Base Information

Chemical Name:5'-O-(tert-butyldimethylsilyl)-N⁶-(4-methoxytrityl)-2'-C-methyladenosine
CAS No.:1390625-38-3
Molecular Formula:C₃₇H₄₅N₅O₅Si
Molecular Weight:667.88
Hs Code.:

5'-O-(tert-butyldimethylsilyl)-N<SUP>6</SUP>-(4-methoxytrityl)-2'-C-methyladenosine

Synonyms:5'-O-(tert-butyldimethylsilyl)-N⁶-(4-methoxytrityl)-2'-C-methyladenosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5'-O-(tert-butyldimethylsilyl)-N⁶-(4-methoxytrityl)-2'-C-methyladenosine

Chemical Property:

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Technology Process of 5'-O-(tert-butyldimethylsilyl)-N⁶-(4-methoxytrityl)-2'-C-methyladenosine

There total 3 articles about 5'-O-(tert-butyldimethylsilyl)-N⁶-(4-methoxytrityl)-2'-C-methyladenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 5'-O-(tert-butyldimethylsilyl)-2'-C-methyladenosine

: 14470-28-1
mono-4-methoxytrityl chloride

: 1390625-38-3
5'-O-(tert-butyldimethylsilyl)-N⁶-(4-methoxytrityl)-2'-C-methyladenosine

Guidance literature:: With pyridine; at 51 ℃; for 17h;
DOI:10.3998/ark.5550190.0013.520

Reference yield:

: 15397-12-3
2'-C-methyladenosine

: 1390625-38-3
5'-O-(tert-butyldimethylsilyl)-N⁶-(4-methoxytrityl)-2'-C-methyladenosine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 18 h / 20 °C

2: pyridine / 17 h / 51 °C

With pyridine;
DOI:10.3998/ark.5550190.0013.520

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1390625-38-3
5'-O-(tert-butyldimethylsilyl)-N⁶-(4-methoxytrityl)-2'-C-methyladenosine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 18 h / 20 °C

2: pyridine / 17 h / 51 °C

With pyridine;
DOI:10.3998/ark.5550190.0013.520