(R)-(-)-3-<(N-methyl-N-trifluoromethanesulfonyl)amino>-1-butanol benzoate

Base Information

Chemical Name:(R)-(-)-3-<(N-methyl-N-trifluoromethanesulfonyl)amino>-1-butanol benzoate
CAS No.:129990-96-1
Molecular Formula:C₁₃H₁₆F₃NO₄S
Molecular Weight:339.336
Hs Code.:

Synonyms:(R)-(-)-3-<(N-methyl-N-trifluoromethanesulfonyl)amino>-1-butanol benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-(-)-3-<(N-methyl-N-trifluoromethanesulfonyl)amino>-1-butanol benzoate

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Technology Process of (R)-(-)-3-<(N-methyl-N-trifluoromethanesulfonyl)amino>-1-butanol benzoate

There total 2 articles about (R)-(-)-3-<(N-methyl-N-trifluoromethanesulfonyl)amino>-1-butanol benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 34310-29-7
N-methyltrifluoromethanesulfonamide

: 82659-86-7
(S)-(+)-1,3-butanediol 1-benzoate

: 129990-96-1
(R)-(-)-3-<(N-methyl-N-trifluoromethanesulfonyl)amino>-1-butanol benzoate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; for 0.166667h;
DOI:10.1016/S0040-4039(00)97411-2

Reference yield:

: 98-88-4
benzoyl chloride

: 129990-96-1
(R)-(-)-3-<(N-methyl-N-trifluoromethanesulfonyl)amino>-1-butanol benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂ / 3 h / -40 °C

2: DEAD, PPh₃ / tetrahydrofuran / 0.5 h

With pyridine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(01)85630-1