3-(3,5-Dimethoxy-phenyl)-1-((1R,5S,7S)-10,10-dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1,5]dec-4-yl)-propan-1-one

Base Information

• Chemical Name: 3-(3,5-Dimethoxy-phenyl)-1-((1R,5S,7S)-10,10-dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1,5]dec-4-yl)-propan-1-one
• CAS No.: 873428-37-6
• Molecular Formula: C₂₁H₂₉NO₅S
• Molecular Weight: 407.531

Synonyms:3-(3,5-Dimethoxy-phenyl)-1-((1R,5S,7S)-10,10-dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1,5]dec-4-yl)-propan-1-one

Chemical Property of 3-(3,5-Dimethoxy-phenyl)-1-((1R,5S,7S)-10,10-dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1,5]dec-4-yl)-propan-1-one

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Technology Process of 3-(3,5-Dimethoxy-phenyl)-1-((1R,5S,7S)-10,10-dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1,5]dec-4-yl)-propan-1-one

There total 3 articles about 3-(3,5-Dimethoxy-phenyl)-1-((1R,5S,7S)-10,10-dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1,5]dec-4-yl)-propan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-3-(3,5-Dimethoxy-phenyl)-1-((1R,5S,7S)-10,10-dimethyl-3,3-dioxo-3λ6-thia-4-aza-tricyclo[5.2.1.01,5]dec-4-yl)-propenone → 3-(3,5-Dimethoxy-phenyl)-1-((1R,5S,7S)-10,10-dimethyl-3,3-dioxo-3λ6-thia-4-aza-tricyclo[5.2.1.01,5]dec-4-yl)-propan-1-one (873428-37-6)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate;

DOI:10.1016/j.bmc.2005.08.013

Reference yield:

(+)-camphorsultam (108448-77-7,124224-04-0) → 3-(3,5-Dimethoxy-phenyl)-1-((1R,5S,7S)-10,10-dimethyl-3,3-dioxo-3λ6-thia-4-aza-tricyclo[5.2.1.01,5]dec-4-yl)-propan-1-one (873428-37-6)

Guidance literature:

Multi-step reaction with 2 steps

1: NaH / toluene / 0 - 25 °C

2: H₂ / Pd-C / ethyl acetate

With hydrogen; sodium hydride; palladium on activated charcoal; In ethyl acetate; toluene;

DOI:10.1016/j.bmc.2005.08.013

Reference yield:

trans-3,5-dimethoxycinnamoyl chloride (195617-72-2) → 3-(3,5-Dimethoxy-phenyl)-1-((1R,5S,7S)-10,10-dimethyl-3,3-dioxo-3λ6-thia-4-aza-tricyclo[5.2.1.01,5]dec-4-yl)-propan-1-one (873428-37-6)

Guidance literature:

Multi-step reaction with 2 steps

1: NaH / toluene / 0 - 25 °C

2: H₂ / Pd-C / ethyl acetate

With hydrogen; sodium hydride; palladium on activated charcoal; In ethyl acetate; toluene;

DOI:10.1016/j.bmc.2005.08.013

upstream raw materials:

(+)-camphorsultam

trans-3,5-dimethoxycinnamoyl chloride

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