(2S,3R)-2-Benzyloxymethoxy-3-(tert-butyl-dimethyl-silanyloxy)-butyraldehyde

Base Information

Chemical Name:(2S,3R)-2-Benzyloxymethoxy-3-(tert-butyl-dimethyl-silanyloxy)-butyraldehyde
CAS No.:132916-22-4
Molecular Formula:C₁₈H₃₀O₄Si
Molecular Weight:338.519
Hs Code.:

Synonyms:(2S,3R)-2-Benzyloxymethoxy-3-(tert-butyl-dimethyl-silanyloxy)-butyraldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R)-2-Benzyloxymethoxy-3-(tert-butyl-dimethyl-silanyloxy)-butyraldehyde

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Technology Process of (2S,3R)-2-Benzyloxymethoxy-3-(tert-butyl-dimethyl-silanyloxy)-butyraldehyde

There total 1 articles about (2S,3R)-2-Benzyloxymethoxy-3-(tert-butyl-dimethyl-silanyloxy)-butyraldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 132916-20-2
(2R,3S)-2-Benzyloxymethoxy-3-(tert-butyl-dimethyl-silanyloxy)-1-(dimethyl-phenyl-silanyl)-butan-1-one

: 132916-22-4
(2S,3R)-2-Benzyloxymethoxy-3-(tert-butyl-dimethyl-silanyloxy)-butyraldehyde

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 10h; under 760 Torr; Ambient temperature;
DOI:10.1016/S0040-4039(00)79467-6

Reference yield:

: 1826-67-1
vinyl magnesium bromide

: 132916-22-4
(2S,3R)-2-Benzyloxymethoxy-3-(tert-butyl-dimethyl-silanyloxy)-butyraldehyde

: 132916-26-8,133005-19-3
(3R,4R,5R)-4-Benzyloxymethoxy-5-(tert-butyl-dimethyl-silanyloxy)-hex-1-en-3-ol

: 132916-26-8,133005-19-3
(3S,4R,5R)-4-Benzyloxymethoxy-5-(tert-butyl-dimethyl-silanyloxy)-hex-1-en-3-ol

Guidance literature:: In dichloromethane; at -78 ℃; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/S0040-4039(00)79467-6