(E)-N'-(1-(5-azido-1H-indol-2-yl)ethylidene)-5-bromo-2-(prop-2-ynyloxy)benzohydrazide

Base Information

Chemical Name:(E)-N'-(1-(5-azido-1H-indol-2-yl)ethylidene)-5-bromo-2-(prop-2-ynyloxy)benzohydrazide
CAS No.:1373438-66-4
Molecular Formula:C₂₀H₁₅BrN₆O₂
Molecular Weight:451.282
Hs Code.:

Synonyms:(E)-N'-(1-(5-azido-1H-indol-2-yl)ethylidene)-5-bromo-2-(prop-2-ynyloxy)benzohydrazide

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Chemical Property of (E)-N'-(1-(5-azido-1H-indol-2-yl)ethylidene)-5-bromo-2-(prop-2-ynyloxy)benzohydrazide

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Technology Process of (E)-N'-(1-(5-azido-1H-indol-2-yl)ethylidene)-5-bromo-2-(prop-2-ynyloxy)benzohydrazide

There total 4 articles about (E)-N'-(1-(5-azido-1H-indol-2-yl)ethylidene)-5-bromo-2-(prop-2-ynyloxy)benzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₀H₆BrClO₂

: C₁₀H₁₀N₆

: 1373438-66-4
(E)-N'-(1-(5-azido-1H-indol-2-yl)ethylidene)-5-bromo-2-(prop-2-ynyloxy)benzohydrazide

Guidance literature:: In dichloromethane; at 0 - 20 ℃; for 2h;

Reference yield:

: 62176-25-4
5-bromo-2-(prop-2-ynyloxy)benzoic acid

: 1373438-66-4
(E)-N'-(1-(5-azido-1H-indol-2-yl)ethylidene)-5-bromo-2-(prop-2-ynyloxy)benzohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / N,N-dimethyl-formamide / 16 h

2: dichloromethane / 2 h / 0 - 20 °C

With thionyl chloride; N,N-dimethyl-formamide; In dichloromethane;

Reference yield:

: 89671-83-0
1-(5-bromo-1H-indol-2-yl)ethan-1-one

: 1373438-66-4
(E)-N'-(1-(5-azido-1H-indol-2-yl)ethylidene)-5-bromo-2-(prop-2-ynyloxy)benzohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide; sodium hydroxide; copper(l) iodide; rac-Pro-OH / ethanol; water / 72 h / 95 °C / Sealed tube

2: hydrazine hydrate / acetic acid / ethanol / 3 h / Reflux

3: dichloromethane / 2 h / 0 - 20 °C

With copper(l) iodide; sodium azide; hydrazine hydrate; rac-Pro-OH; sodium hydroxide; acetic acid; In ethanol; dichloromethane; water;