methyl (1S,3aR,4S,5R,7aS)-1-ethyl-3a,4,5,7a-tetrahydro-5-<(phenylthio)methyl>-4-indancarboxylate

Base Information

Chemical Name:methyl (1S,3aR,4S,5R,7aS)-1-ethyl-3a,4,5,7a-tetrahydro-5-<(phenylthio)methyl>-4-indancarboxylate
CAS No.:95532-30-2
Molecular Formula:C₂₀H₂₆O₂S
Molecular Weight:330.491
Hs Code.:

Synonyms:methyl (1S,3aR,4S,5R,7aS)-1-ethyl-3a,4,5,7a-tetrahydro-5-<(phenylthio)methyl>-4-indancarboxylate

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Chemical Property of methyl (1S,3aR,4S,5R,7aS)-1-ethyl-3a,4,5,7a-tetrahydro-5-<(phenylthio)methyl>-4-indancarboxylate

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Technology Process of methyl (1S,3aR,4S,5R,7aS)-1-ethyl-3a,4,5,7a-tetrahydro-5-<(phenylthio)methyl>-4-indancarboxylate

There total 18 articles about methyl (1S,3aR,4S,5R,7aS)-1-ethyl-3a,4,5,7a-tetrahydro-5-<(phenylthio)methyl>-4-indancarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 81331-47-7,95671-28-6
(+/-)-(1S,3aR,4S,5R,7aS)-1-ethyl-3a,4,5,7a-tetrahydro-5-<(phenylthio)methyl>-4-indancarboxylic acid

: 95532-30-2
(+/-)-methyl (1S,3aR,4S,5R,7aS)-1-ethyl-3a,4,5,7a-tetrahydro-5-<(phenylthio)methyl>-4-indancarboxylate

Guidance literature:: In diethyl ether; at 0 ℃;
DOI:10.1021/ja00413a037 DOI:10.1021/jo00209a017

Reference yield:

: 2973-86-6
lithium thiophenoxide

: 95532-30-2
(+/-)-methyl (1S,3aR,4S,5R,7aS)-1-ethyl-3a,4,5,7a-tetrahydro-5-<(phenylthio)methyl>-4-indancarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylformamide / 3 h / 110 °C

2: diethyl ether / 0 °C

In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/ja00413a037 DOI:10.1021/jo00209a017

Reference yield:

: 76566-89-7,88244-69-3,78216-75-8,91109-68-1
(+/-)-1α-Ethyl-5β-(hydroxymethyl)-3aβ,4,5,7aα-tetrahydroindan-4β-carboxylic Acid γ-Lactone

: 95532-30-2
(+/-)-methyl (1S,3aR,4S,5R,7aS)-1-ethyl-3a,4,5,7a-tetrahydro-5-<(phenylthio)methyl>-4-indancarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylformamide / 3 h / 110 °C

2: diethyl ether / 0 °C

In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/ja00413a037 DOI:10.1021/jo00209a017