C₁₀H₁₂N₄S

Base Information

Chemical Name:C₁₀H₁₂N₄S
CAS No.:145083-94-9
Molecular Formula:C₁₀H₁₂N₄S
Molecular Weight:220.298
Hs Code.:

C<sub>10</sub>H<sub>12</sub>N<sub>4</sub>S

Synonyms:C₁₀H₁₂N₄S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₀H₁₂N₄S

Chemical Property:

Purity/Quality:

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Technology Process of C₁₀H₁₂N₄S

There total 5 articles about C₁₀H₁₂N₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22901-09-3
2-(2-bromoethyl)benzaldehyde

: 145083-94-9
C₁₀H₁₂N₄S

Guidance literature:: Multi-step reaction with 5 steps

1: 94 percent / sodium azide, sodium iodide / dimethylsulfoxide / 105 °C

2: 83 percent / aq. hydroxylamine hydrochloride, sodium carbonate / ethanol / 1 h / Heating

3: 1.) acetic anhydride, sodium acetate, 2.) triethylamine / 1.) 110 deg C, 2 h, 2.) toluene, heating, overnight

4: triphenylphosphine / 3 h / Heating

5: 50 percent aq. hydrazine / ethanol / 1 h

With sodium azide; hydroxylamine hydrochloride; sodium acetate; acetic anhydride; sodium carbonate; hydrazine hydrate; triethylamine; triphenylphosphine; sodium iodide; In ethanol; dimethyl sulfoxide;
DOI:10.1016/S0040-4020(01)90364-3

Reference yield:

: 2-(2-Isothiocyanato-ethyl)-benzonitrile

: 145083-94-9
C₁₀H₁₂N₄S

Guidance literature:: With hydrazine hydrate; In ethanol; for 1h; Yield given;
DOI:10.1016/S0040-4020(01)90364-3

Reference yield:

: 145083-91-6
2-(2-azidoethyl)benzaldehyde

: 145083-94-9
C₁₀H₁₂N₄S

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / aq. hydroxylamine hydrochloride, sodium carbonate / ethanol / 1 h / Heating

2: 1.) acetic anhydride, sodium acetate, 2.) triethylamine / 1.) 110 deg C, 2 h, 2.) toluene, heating, overnight

3: triphenylphosphine / 3 h / Heating

4: 50 percent aq. hydrazine / ethanol / 1 h

With hydroxylamine hydrochloride; sodium acetate; acetic anhydride; sodium carbonate; hydrazine hydrate; triethylamine; triphenylphosphine; In ethanol;
DOI:10.1016/S0040-4020(01)90364-3