methyl (2S,3R,4S,5R)-2-(benzyloxy)-4-(dibenzylamino)-6-((4R,5S)-5-(dibenzylamino)-2,2-dimethyl-1,3-dioxan-4-yl)-3-hydroxy-5-(methoxymethoxy)hexanoate

Base Information

Chemical Name:methyl (2S,3R,4S,5R)-2-(benzyloxy)-4-(dibenzylamino)-6-((4R,5S)-5-(dibenzylamino)-2,2-dimethyl-1,3-dioxan-4-yl)-3-hydroxy-5-(methoxymethoxy)hexanoate
CAS No.:1092536-22-5
Molecular Formula:C₅₀H₆₀N₂O₈
Molecular Weight:817.035
Hs Code.:

Synonyms:methyl (2S,3R,4S,5R)-2-(benzyloxy)-4-(dibenzylamino)-6-((4R,5S)-5-(dibenzylamino)-2,2-dimethyl-1,3-dioxan-4-yl)-3-hydroxy-5-(methoxymethoxy)hexanoate

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Chemical Property of methyl (2S,3R,4S,5R)-2-(benzyloxy)-4-(dibenzylamino)-6-((4R,5S)-5-(dibenzylamino)-2,2-dimethyl-1,3-dioxan-4-yl)-3-hydroxy-5-(methoxymethoxy)hexanoate

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Technology Process of methyl (2S,3R,4S,5R)-2-(benzyloxy)-4-(dibenzylamino)-6-((4R,5S)-5-(dibenzylamino)-2,2-dimethyl-1,3-dioxan-4-yl)-3-hydroxy-5-(methoxymethoxy)hexanoate

There total 1 articles about methyl (2S,3R,4S,5R)-2-(benzyloxy)-4-(dibenzylamino)-6-((4R,5S)-5-(dibenzylamino)-2,2-dimethyl-1,3-dioxan-4-yl)-3-hydroxy-5-(methoxymethoxy)hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1092536-11-2
(2R,3R)-2-(dibenzylamino)-4-((4R,5S)-5-(dibenzylamino)-2,2-dimethyl-1,3-dioxan-4-yl)-3-(methoxymethoxy)butanal

: 31600-43-8
methyl 2-(benzyloxy)acetate

: 1092536-22-5
methyl (2S,3R,4S,5R)-2-(benzyloxy)-4-(dibenzylamino)-6-((4R,5S)-5-(dibenzylamino)-2,2-dimethyl-1,3-dioxan-4-yl)-3-hydroxy-5-(methoxymethoxy)hexanoate

Guidance literature:: methyl 2-(benzyloxy)acetate; With di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine; In diethyl ether; at -78 ℃; for 1.5h; Inert atmosphere;

(2R,3R)-2-(dibenzylamino)-4-((4R,5S)-5-(dibenzylamino)-2,2-dimethyl-1,3-dioxan-4-yl)-3-(methoxymethoxy)butanal; In diethyl ether; at -78 - 0 ℃; Inert atmosphere;

With dihydrogen peroxide; In methanol; diethyl ether; at 0 ℃; for 1h; pH=7; optical yield given as %de; aq. phosphate buffer;
DOI:10.1002/anie.200801561

Reference yield: 81.0%

: 1092536-22-5
methyl (2S,3R,4S,5R)-2-(benzyloxy)-4-(dibenzylamino)-6-((4R,5S)-5-(dibenzylamino)-2,2-dimethyl-1,3-dioxan-4-yl)-3-hydroxy-5-(methoxymethoxy)hexanoate

: 1092536-12-3
(2S,3R,4S,5R)-2-(benzyloxy)-4-(dibenzylamino)-6-((4R,5S)-5-(dibenzylamino)-2,2-dimethyl-1,3-dioxan-4-yl)-3-hydroxy-5-(methoxymethoxy)hexanoic acid

Guidance literature:: methyl (2S,3R,4S,5R)-2-(benzyloxy)-4-(dibenzylamino)-6-((4R,5S)-5-(dibenzylamino)-2,2-dimethyl-1,3-dioxan-4-yl)-3-hydroxy-5-(methoxymethoxy)hexanoate; With lithium hydroxide monohydrate; In tetrahydrofuran; methanol; water; at 20 ℃; for 8h;

With hydrogenchloride; In tetrahydrofuran; methanol; water; pH=2;
DOI:10.1002/anie.200801561