(2S,5S)-1-[2-(dicyclohexylphosphino)benzylideneamino]-2,5-diphenylpyrrolidine

Base Information

Chemical Name:(2S,5S)-1-[2-(dicyclohexylphosphino)benzylideneamino]-2,5-diphenylpyrrolidine
CAS No.:1374113-96-8
Molecular Formula:C₃₅H₄₃N₂P
Molecular Weight:522.714
Hs Code.:

Synonyms:(2S,5S)-1-[2-(dicyclohexylphosphino)benzylideneamino]-2,5-diphenylpyrrolidine

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Chemical Property of (2S,5S)-1-[2-(dicyclohexylphosphino)benzylideneamino]-2,5-diphenylpyrrolidine

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Technology Process of (2S,5S)-1-[2-(dicyclohexylphosphino)benzylideneamino]-2,5-diphenylpyrrolidine

There total 7 articles about (2S,5S)-1-[2-(dicyclohexylphosphino)benzylideneamino]-2,5-diphenylpyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1374113-95-7
(2S,5S)-1-[2-(dicyclohexylphosphoryl)benzylideneamino]-2,5-diphenylpyrrolidine

: 1374113-96-8
(2S,5S)-1-[2-(dicyclohexylphosphino)benzylideneamino]-2,5-diphenylpyrrolidine

Guidance literature:: With trichlorosilane; triethylamine; In toluene; at 110 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jo300548z

Reference yield:

: 34824-58-3
2-(2-bromophenyl)-1,3-dioxolan

: 1374113-96-8
(2S,5S)-1-[2-(dicyclohexylphosphino)benzylideneamino]-2,5-diphenylpyrrolidine

Guidance literature:: Multi-step reaction with 4 steps

1.1: tert.-butyl lithium / diethyl ether / -78 °C

1.2: -78 - 20 °C

2.1: water; toluene-4-sulfonic acid; acetone / Reflux

3.1: toluene / 3 h / 20 °C

4.1: trichlorosilane; triethylamine / toluene / 24 h / 110 °C / Inert atmosphere

With trichlorosilane; water; tert.-butyl lithium; toluene-4-sulfonic acid; triethylamine; acetone; In diethyl ether; toluene;
DOI:10.1021/jo300548z

Reference yield:

: C₂₁H₃₁O₃P

: 1374113-96-8
(2S,5S)-1-[2-(dicyclohexylphosphino)benzylideneamino]-2,5-diphenylpyrrolidine

Guidance literature:: Multi-step reaction with 3 steps

1: water; toluene-4-sulfonic acid; acetone / Reflux

2: toluene / 3 h / 20 °C

3: trichlorosilane; triethylamine / toluene / 24 h / 110 °C / Inert atmosphere

With trichlorosilane; water; toluene-4-sulfonic acid; triethylamine; acetone; In toluene;
DOI:10.1021/jo300548z