tert-Butyl-dimethyl-[(2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-((1R,2S,6S,7R,8R)-4,4-dimethyl-3,5,9,11-tetraoxa-tricyclo[6.2.1.0^2,6]undec-7-yloxy)-tetrahydro-pyran-2-ylmethoxy]-silane

Base Information

• Chemical Name: tert-Butyl-dimethyl-[(2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-((1R,2S,6S,7R,8R)-4,4-dimethyl-3,5,9,11-tetraoxa-tricyclo[6.2.1.0^2,6]undec-7-yloxy)-tetrahydro-pyran-2-ylmethoxy]-silane
• CAS No.: 131622-47-4
• Molecular Formula: C₄₂H₅₆O₁₀Si
• Molecular Weight: 748.986

Synonyms:tert-Butyl-dimethyl-[(2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-((1R,2S,6S,7R,8R)-4,4-dimethyl-3,5,9,11-tetraoxa-tricyclo[6.2.1.0^2,6]undec-7-yloxy)-tetrahydro-pyran-2-ylmethoxy]-silane

Chemical Property of tert-Butyl-dimethyl-[(2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-((1R,2S,6S,7R,8R)-4,4-dimethyl-3,5,9,11-tetraoxa-tricyclo[6.2.1.0^2,6]undec-7-yloxy)-tetrahydro-pyran-2-ylmethoxy]-silane

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Technology Process of tert-Butyl-dimethyl-[(2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-((1R,2S,6S,7R,8R)-4,4-dimethyl-3,5,9,11-tetraoxa-tricyclo[6.2.1.0^2,6]undec-7-yloxy)-tetrahydro-pyran-2-ylmethoxy]-silane

There total 1 articles about tert-Butyl-dimethyl-[(2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-((1R,2S,6S,7R,8R)-4,4-dimethyl-3,5,9,11-tetraoxa-tricyclo[6.2.1.0^2,6]undec-7-yloxy)-tetrahydro-pyran-2-ylmethoxy]-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C43H60N3O5PSSi (130738-58-8) + 1,6-anhydro-3,4-O-isopropylidene-β-D-galactopyranose (52579-97-2) → tert-Butyl-dimethyl-[(2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-((1R,2S,6S,7R,8R)-4,4-dimethyl-3,5,9,11-tetraoxa-tricyclo[6.2.1.02,6]undec-7-yloxy)-tetrahydro-pyran-2-ylmethoxy]-silane (130738-63-5) + tert-Butyl-dimethyl-[(2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-((1R,2S,6S,7R,8R)-4,4-dimethyl-3,5,9,11-tetraoxa-tricyclo[6.2.1.02,6]undec-7-yloxy)-tetrahydro-pyran-2-ylmethoxy]-silane (131622-47-4)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; 2,6-lutidinium p-toluenesulfonate; 4 A molecular sieve; In toluene; at 23 ℃; for 55h; Yield given. Yields of byproduct given;

DOI:10.1016/S0040-4039(00)97729-3

upstream raw materials:

C₄₃H₆₀N₃O₅PSSi

1,6-anhydro-3,4-O-isopropylidene-β-D-galactopyranose

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