benzyl N-(3-ethyloxetan-3-yl)carbamate

Base Information

• Chemical Name: benzyl N-(3-ethyloxetan-3-yl)carbamate
• CAS No.: 1365969-56-7
• Molecular Formula: C₁₃H₁₇NO₃
• Molecular Weight: 235.283
• Hs Code.: 2932990090
• Mol file: 1365969-56-7.mol

Synonyms:benzyl N-(3-ethyloxetan-3-yl)carbamate

Chemical Property of benzyl N-(3-ethyloxetan-3-yl)carbamate

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

BenzylN-(3-ethyloxetan-3-yl)carbamate 95%+ ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzyl N-(3-ethyloxetan-3-yl)carbamate

There total 1 articles about benzyl N-(3-ethyloxetan-3-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-ethyloxetane-3-carboxylic acid (28562-61-0) + benzyl alcohol (100-51-6,185532-71-2) → benzyl N-(3-ethyloxetan-3-yl)carbamate (1365969-56-7)

Guidance literature:

With diphenyl phosphoryl azide; triethylamine; In toluene; at 110 ℃;

Reference yield:

benzyl N-(3-ethyloxetan-3-yl)carbamate (1365969-56-7) → C19H21FN2O4S (1572510-65-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: cyclohexa-1,4-diene; palladium 10% on activated carbon; hydrogen / methanol / 4 h / 25 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 25 °C

2.2: 1 h

With cyclohexa-1,4-diene; palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;

upstream raw materials:

3-ethyloxetane-3-carboxylic acid

benzyl alcohol

Downstream raw materials:

C₁₉H₂₁FN₂O₄S