C₅₁H₅₅NO₁₅

Base Information

Chemical Name:C₅₁H₅₅NO₁₅
CAS No.:360075-34-9
Molecular Formula:C₅₁H₅₅NO₁₅
Molecular Weight:921.995
Hs Code.:

C<sub>51</sub>H<sub>55</sub>NO<sub>15</sub>

Synonyms:C₅₁H₅₅NO₁₅

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Chemical Property of C₅₁H₅₅NO₁₅

Chemical Property:

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Technology Process of C₅₁H₅₅NO₁₅

There total 16 articles about C₅₁H₅₅NO₁₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40359-32-8
3-allyloxy-benzaldehyde

: 360075-34-9
C₅₁H₅₅NO₁₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: MgSO₄ / CH₂Cl₂ / 12 h

2.1: 75 percent / i-Pr₂NEt / CH₂Cl₂ / 12 h / -78 - 20 °C

3.1: 48 percent / lipase PS / aq. phosphate buffer; acetonitrile / 74 h / 20 °C / pH 7

4.1: 99 percent / aq. KOH / tetrahydrofuran / 0.25 h

5.1: 1.15 g / imidazole / dimethylformamide / 8 h / 20 °C

6.1: 78 percent / aq. ceric ammonium nitrate / acetonitrile / 1.08 h / 0 °C

7.1: 82 percent / dimethylaminopyridine / CH₂Cl₂ / 1 h / 0 °C

8.1: NaH / tetrahydrofuran / 0.25 h / 0 °C

8.2: 62 percent / tetrahydrofuran / 24 h / 0 - 20 °C

9.1: 85 percent / (PCy₃)2(Cl)2Ru=CHPh / CH₂Cl₂ / 20 °C

10.1: 75 percent / HF*pyridine / tetrahydrofuran / 0 - 20 °C

With 1H-imidazole; dmap; potassium hydroxide; ammonium cerium(IV) nitrate; Lipase PS; sodium hydride; magnesium sulfate; pyridine hydrogenfluoride; N-ethyl-N,N-diisopropylamine; Grubbs catalyst first generation; In tetrahydrofuran; phosphate buffer; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm061071x

Reference yield:

: 39716-58-0
pent-4-enoyl chloride

: 360075-34-9
C₅₁H₅₅NO₁₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium hexamethyldisilazide / tetrahydrofuran / 0.75 h / 0 °C

1.2: 78 percent / tetrahydrofuran / 3 h / 0 °C

2.1: 91 percent / HF*pyridine / tetrahydrofuran / 24 h / 0 - 20 °C

3.1: 92 percent / CeCl₃ / tetrahydrofuran / 4 h

4.1: 85 percent / imidazole / CH₂Cl₂ / 3 h / 0 °C

5.1: NaH / tetrahydrofuran / 0.25 h / 0 °C

5.2: 62 percent / tetrahydrofuran / 24 h / 0 - 20 °C

6.1: 85 percent / (PCy₃)2(Cl)2Ru=CHPh / CH₂Cl₂ / 20 °C

7.1: 75 percent / HF*pyridine / tetrahydrofuran / 0 - 20 °C

With 1H-imidazole; cerium(III) chloride; sodium hydride; pyridine hydrogenfluoride; lithium hexamethyldisilazane; Grubbs catalyst first generation; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm061071x

Reference yield:

: (rac)-(3RS,4SR)-1-(p-methoxyphenyl)-3-acetyloxy-4-(m-allyloxyphenyl)azetidin-2-one

: 360075-34-9
C₅₁H₅₅NO₁₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: 48 percent / lipase PS / aq. phosphate buffer; acetonitrile / 74 h / 20 °C / pH 7

2.1: 99 percent / aq. KOH / tetrahydrofuran / 0.25 h

3.1: 1.15 g / imidazole / dimethylformamide / 8 h / 20 °C

4.1: 78 percent / aq. ceric ammonium nitrate / acetonitrile / 1.08 h / 0 °C

5.1: 82 percent / dimethylaminopyridine / CH₂Cl₂ / 1 h / 0 °C

6.1: NaH / tetrahydrofuran / 0.25 h / 0 °C

6.2: 62 percent / tetrahydrofuran / 24 h / 0 - 20 °C

7.1: 85 percent / (PCy₃)2(Cl)2Ru=CHPh / CH₂Cl₂ / 20 °C

8.1: 75 percent / HF*pyridine / tetrahydrofuran / 0 - 20 °C

With 1H-imidazole; dmap; potassium hydroxide; ammonium cerium(IV) nitrate; Lipase PS; sodium hydride; pyridine hydrogenfluoride; Grubbs catalyst first generation; In tetrahydrofuran; phosphate buffer; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm061071x