5-[Ethyl-(2-methanesulfonyloxy-ethyl)-amino]-2,4-dinitro-benzoic acid methyl ester

Base Information

• Chemical Name: 5-[Ethyl-(2-methanesulfonyloxy-ethyl)-amino]-2,4-dinitro-benzoic acid methyl ester
• CAS No.: 1027283-98-2
• Molecular Formula: C₁₃H₁₇N₃O₉S
• Molecular Weight: 391.359

Synonyms:5-[Ethyl-(2-methanesulfonyloxy-ethyl)-amino]-2,4-dinitro-benzoic acid methyl ester

Chemical Property of 5-[Ethyl-(2-methanesulfonyloxy-ethyl)-amino]-2,4-dinitro-benzoic acid methyl ester

Chemical Property:

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Technology Process of 5-[Ethyl-(2-methanesulfonyloxy-ethyl)-amino]-2,4-dinitro-benzoic acid methyl ester

There total 2 articles about 5-[Ethyl-(2-methanesulfonyloxy-ethyl)-amino]-2,4-dinitro-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanesulfonyl chloride (124-63-0) + methyl 2,4-dinitro-5-benzoate (156423-06-2) → 5-[Ethyl-(2-methanesulfonyloxy-ethyl)-amino]-2,4-dinitro-benzoic acid methyl ester (1027283-98-2)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1021/jm00040a009

Reference yield:

methyl 5-chloro-2,4-dinitrobenzoate (150272-08-5) → 5-[Ethyl-(2-methanesulfonyloxy-ethyl)-amino]-2,4-dinitro-benzoic acid methyl ester (1027283-98-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 89 percent / dioxane / 8 h / 20 °C

2: Et₃N / CH₂Cl₂ / 0.5 h / 20 °C

With triethylamine; In 1,4-dioxane; dichloromethane;

DOI:10.1021/jm00040a009

Reference yield:

5-[Ethyl-(2-methanesulfonyloxy-ethyl)-amino]-2,4-dinitro-benzoic acid methyl ester (1027283-98-2) → methyl 5--2,4-dinitrobenzoate (156423-07-3)

Guidance literature:

With lithium chloride; In N,N-dimethyl-formamide; at 80 ℃; for 0.25h; Yield given;

DOI:10.1021/jm00040a009

upstream raw materials:

methanesulfonyl chloride

methyl 2,4-dinitro-5-benzoate

methyl 5-chloro-2,4-dinitrobenzoate

Downstream raw materials:

methyl 5--2,4-dinitrobenzoate

5--2,4-dinitrobenzoic acid

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