2-O-benzoyl-3,6-di-O-benzyl-4-O-tert-butyldimethylsilyl-α-D-mannopyranose

Base Information

Chemical Name:2-O-benzoyl-3,6-di-O-benzyl-4-O-tert-butyldimethylsilyl-α-D-mannopyranose
CAS No.:351011-71-7
Molecular Formula:C₃₃H₄₂O₇Si
Molecular Weight:578.778
Hs Code.:

Synonyms:2-O-benzoyl-3,6-di-O-benzyl-4-O-tert-butyldimethylsilyl-α-D-mannopyranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-O-benzoyl-3,6-di-O-benzyl-4-O-tert-butyldimethylsilyl-α-D-mannopyranose

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Technology Process of 2-O-benzoyl-3,6-di-O-benzyl-4-O-tert-butyldimethylsilyl-α-D-mannopyranose

There total 5 articles about 2-O-benzoyl-3,6-di-O-benzyl-4-O-tert-butyldimethylsilyl-α-D-mannopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 351011-56-8
p-methoxyphenyl 2-O-benzoyl-3,6-di-O-benzyl-4-O-tert-butyldimethylsilyl-α-D-mannopyranosyde

: 351011-71-7
2-O-benzoyl-3,6-di-O-benzyl-4-O-tert-butyldimethylsilyl-α-D-mannopyranose

Guidance literature:: With ammonium cerium(IV) nitrate; In acetonitrile; at 20 ℃; for 0.166667h;
DOI:10.1021/jo015521z

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 351011-71-7
2-O-benzoyl-3,6-di-O-benzyl-4-O-tert-butyldimethylsilyl-α-D-mannopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / 2,6-lutidine / CH₂Cl₂ / 0.33 h

2: 99 percent / aq. cerium ammonium nitrate / acetonitrile / 0.17 h / 20 °C

With 2,6-dimethylpyridine; ammonium cerium(IV) nitrate; In dichloromethane; acetonitrile;
DOI:10.1021/jo015521z

Reference yield:

: 123826-52-8
p-methoxyphenyl 3,6-di-O-benzyl-α-D-mannopyranoside

: 351011-71-7
2-O-benzoyl-3,6-di-O-benzyl-4-O-tert-butyldimethylsilyl-α-D-mannopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / pyridine / 0.25 h / -20 °C

2: 96 percent / 2,6-lutidine / CH₂Cl₂ / 0.33 h

3: 99 percent / aq. cerium ammonium nitrate / acetonitrile / 0.17 h / 20 °C

With pyridine; 2,6-dimethylpyridine; ammonium cerium(IV) nitrate; In dichloromethane; acetonitrile;
DOI:10.1021/jo015521z