p-methoxyphenyl 2-O-benzoyl-3,6-di-O-benzyl-4-O-tert-butyldimethylsilyl-α-D-mannopyranosyde

Base Information

Chemical Name:p-methoxyphenyl 2-O-benzoyl-3,6-di-O-benzyl-4-O-tert-butyldimethylsilyl-α-D-mannopyranosyde
CAS No.:351011-56-8
Molecular Formula:C₄₀H₄₈O₈Si
Molecular Weight:684.902
Hs Code.:

Synonyms:p-methoxyphenyl 2-O-benzoyl-3,6-di-O-benzyl-4-O-tert-butyldimethylsilyl-α-D-mannopyranosyde

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Chemical Property of p-methoxyphenyl 2-O-benzoyl-3,6-di-O-benzyl-4-O-tert-butyldimethylsilyl-α-D-mannopyranosyde

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Technology Process of p-methoxyphenyl 2-O-benzoyl-3,6-di-O-benzyl-4-O-tert-butyldimethylsilyl-α-D-mannopyranosyde

There total 3 articles about p-methoxyphenyl 2-O-benzoyl-3,6-di-O-benzyl-4-O-tert-butyldimethylsilyl-α-D-mannopyranosyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 69739-34-0
t-butyldimethylsiyl triflate

: 351011-70-6,1393898-89-9
p-methoxyphenyl 2-O-benzoyl-3,6-di-O-benzyl-α-D-mannopyranosyde

: 351011-56-8
p-methoxyphenyl 2-O-benzoyl-3,6-di-O-benzyl-4-O-tert-butyldimethylsilyl-α-D-mannopyranosyde

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; for 0.333333h;
DOI:10.1021/jo015521z

Reference yield:

: 123826-52-8
p-methoxyphenyl 3,6-di-O-benzyl-α-D-mannopyranoside

: 351011-56-8
p-methoxyphenyl 2-O-benzoyl-3,6-di-O-benzyl-4-O-tert-butyldimethylsilyl-α-D-mannopyranosyde

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / pyridine / 0.25 h / -20 °C

2: 96 percent / 2,6-lutidine / CH₂Cl₂ / 0.33 h

With pyridine; 2,6-dimethylpyridine; In dichloromethane;
DOI:10.1021/jo015521z

Reference yield:

: 98-88-4
benzoyl chloride

: 351011-56-8
p-methoxyphenyl 2-O-benzoyl-3,6-di-O-benzyl-4-O-tert-butyldimethylsilyl-α-D-mannopyranosyde

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / pyridine / 0.25 h / -20 °C

2: 96 percent / 2,6-lutidine / CH₂Cl₂ / 0.33 h

With pyridine; 2,6-dimethylpyridine; In dichloromethane;
DOI:10.1021/jo015521z