2-<3-<3-(2-hydroxy-5-methylphenylthio)-2-hydroxy-5-methylphenylthio>-2-hydroxy-5-methylphenylthio>-4-methylphenol

Base Information

Chemical Name:2-<3-<3-(2-hydroxy-5-methylphenylthio)-2-hydroxy-5-methylphenylthio>-2-hydroxy-5-methylphenylthio>-4-methylphenol
CAS No.:133785-82-7
Molecular Formula:C₂₈H₂₆O₄S₃
Molecular Weight:522.71
Hs Code.:

Synonyms:2-<3-<3-(2-hydroxy-5-methylphenylthio)-2-hydroxy-5-methylphenylthio>-2-hydroxy-5-methylphenylthio>-4-methylphenol

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Chemical Property of 2-<3-<3-(2-hydroxy-5-methylphenylthio)-2-hydroxy-5-methylphenylthio>-2-hydroxy-5-methylphenylthio>-4-methylphenol

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Technology Process of 2-<3-<3-(2-hydroxy-5-methylphenylthio)-2-hydroxy-5-methylphenylthio>-2-hydroxy-5-methylphenylthio>-4-methylphenol

There total 3 articles about 2-<3-<3-(2-hydroxy-5-methylphenylthio)-2-hydroxy-5-methylphenylthio>-2-hydroxy-5-methylphenylthio>-4-methylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 2929-96-6
2,2'-thiobis<4-methylphenol>

: 133785-82-7
2-<3-<3-(2-hydroxy-5-methylphenylthio)-2-hydroxy-5-methylphenylthio>-2-hydroxy-5-methylphenylthio>-4-methylphenol

Guidance literature:: With sulfur dichloride; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1246/bcsj.64.576

Reference yield:

: 133785-91-8
2C₂₈H₂₆O₄S₃*C₆H₆

: 133785-82-7
2-<3-<3-(2-hydroxy-5-methylphenylthio)-2-hydroxy-5-methylphenylthio>-2-hydroxy-5-methylphenylthio>-4-methylphenol

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

Guidance literature:: at 117.1 - 132.3 ℃; Rate constant; Kinetics; Thermodynamic data; ΔH(excit.), lnA;
DOI:10.1246/bcsj.64.576

Reference yield:

: 106-44-5
p-cresol

: 133785-82-7
2-<3-<3-(2-hydroxy-5-methylphenylthio)-2-hydroxy-5-methylphenylthio>-2-hydroxy-5-methylphenylthio>-4-methylphenol

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / SCl₂ / CH₂Cl₂

2: 24 percent / SCl₂ / CH₂Cl₂ / 1 h / 0 °C

With sulfur dichloride; In dichloromethane;
DOI:10.1246/bcsj.64.576