benzyl 4-((4-(ethoxylcarbonyl)-4-methylcyclohexyl)oxy)pipereidine-1-carboxylate

Base Information

Chemical Name:benzyl 4-((4-(ethoxylcarbonyl)-4-methylcyclohexyl)oxy)pipereidine-1-carboxylate
CAS No.:1614234-64-8
Molecular Formula:C₂₃H₃₃NO₅
Molecular Weight:403.519
Hs Code.:

Synonyms:benzyl 4-((4-(ethoxylcarbonyl)-4-methylcyclohexyl)oxy)pipereidine-1-carboxylate

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Chemical Property of benzyl 4-((4-(ethoxylcarbonyl)-4-methylcyclohexyl)oxy)pipereidine-1-carboxylate

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Technology Process of benzyl 4-((4-(ethoxylcarbonyl)-4-methylcyclohexyl)oxy)pipereidine-1-carboxylate

There total 3 articles about benzyl 4-((4-(ethoxylcarbonyl)-4-methylcyclohexyl)oxy)pipereidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19099-93-5
benzyl 4-oxo-1-piperidinecarboxylate

: C₁₃H₂₆O₃Si

: 1614234-64-8
benzyl 4-((4-(ethoxylcarbonyl)-4-methylcyclohexyl)oxy)pipereidine-1-carboxylate

Guidance literature:: With triethylsilane; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -60 - 0 ℃; for 0.5h;
DOI:10.1016/j.tet.2014.04.064

Reference yield:

: 147905-77-9
ethyl 1-methyl-4-oxo-1-cyclohexanecarboxylate

: 1614234-64-8
benzyl 4-((4-(ethoxylcarbonyl)-4-methylcyclohexyl)oxy)pipereidine-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: ketoreductase MIF-20; NADP / isopropyl alcohol; aq. phosphate buffer / pH 7 / Enzymatic reaction

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 5 °C

3: triethylsilane; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.5 h / -60 - 0 °C

With triethylsilane; trimethylsilyl trifluoromethanesulfonate; ketoreductase MIF-20; NADP; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; aq. phosphate buffer; dichloromethane; isopropyl alcohol;
DOI:10.1016/j.tet.2014.04.064

Reference yield:

: 1252900-68-7
ethyl 4-hydroxy-1-methylcyclohexanecarboxylate

: 1614234-64-8
benzyl 4-((4-(ethoxylcarbonyl)-4-methylcyclohexyl)oxy)pipereidine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 5 °C

2: triethylsilane; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.5 h / -60 - 0 °C

With triethylsilane; trimethylsilyl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tet.2014.04.064