N-dodecyl-6-O-benzyl-3,4-O-isopropylidene-5a-carba-β-D-galactopyranosylamine

Base Information

Chemical Name:N-dodecyl-6-O-benzyl-3,4-O-isopropylidene-5a-carba-β-D-galactopyranosylamine
CAS No.:828269-04-1
Molecular Formula:C₂₉H₄₉NO₄
Molecular Weight:475.712
Hs Code.:

Synonyms:N-dodecyl-6-O-benzyl-3,4-O-isopropylidene-5a-carba-β-D-galactopyranosylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-dodecyl-6-O-benzyl-3,4-O-isopropylidene-5a-carba-β-D-galactopyranosylamine

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Technology Process of N-dodecyl-6-O-benzyl-3,4-O-isopropylidene-5a-carba-β-D-galactopyranosylamine

There total 1 articles about N-dodecyl-6-O-benzyl-3,4-O-isopropylidene-5a-carba-β-D-galactopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 124-22-1
n-Dodecylamine

: 157609-12-6
1,2-anhydro-6-O-benzyl-3,4-O-isopropylidene-5a-carba-α-D-galactopyranose

: 828269-04-1
N-dodecyl-6-O-benzyl-3,4-O-isopropylidene-5a-carba-β-D-galactopyranosylamine

Guidance literature:: In isopropyl alcohol; at 120 ℃; for 48h;
DOI:10.1016/j.bmc.2004.09.023

Reference yield:

: 828269-04-1
N-dodecyl-6-O-benzyl-3,4-O-isopropylidene-5a-carba-β-D-galactopyranosylamine

: (1S,2S,3S,4R,6R)-4-Benzyloxymethyl-6-dodecylamino-cyclohexane-1,2,3-triol

Guidance literature:: With acetic acid; In water; at 80 ℃; for 16h;
DOI:10.1016/j.bmc.2004.09.023

Reference yield:

: 828269-04-1
N-dodecyl-6-O-benzyl-3,4-O-isopropylidene-5a-carba-β-D-galactopyranosylamine

: N-dodecyl-5a-carba-β-D-galactopyranosylamine

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / H₂O / 16 h / 80 °C

2: 25 mg / hydrogen / palladium on carbon / ethanol / 3 h / 20 °C / atmospheric pressure

With hydrogen; acetic acid; palladium on activated charcoal; In ethanol; water;
DOI:10.1016/j.bmc.2004.09.023