(S)-(-)-N,N,N',N'-tetramethyl-2-<(diphenylphosphino)methyl>pyrrolidinylphosphonic triamide

Base Information

Chemical Name:(S)-(-)-N,N,N',N'-tetramethyl-2-<(diphenylphosphino)methyl>pyrrolidinylphosphonic triamide
CAS No.:145818-30-0
Molecular Formula:C₂₁H₃₁N₃OP₂
Molecular Weight:403.444
Hs Code.:

Synonyms:(S)-(-)-N,N,N',N'-tetramethyl-2-<(diphenylphosphino)methyl>pyrrolidinylphosphonic triamide

Suppliers and Price of (S)-(-)-N,N,N',N'-tetramethyl-2-<(diphenylphosphino)methyl>pyrrolidinylphosphonic triamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-(-)-N,N,N',N'-tetramethyl-2-<(diphenylphosphino)methyl>pyrrolidinylphosphonic triamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-(-)-N,N,N',N'-tetramethyl-2-<(diphenylphosphino)methyl>pyrrolidinylphosphonic triamide

There total 2 articles about (S)-(-)-N,N,N',N'-tetramethyl-2-<(diphenylphosphino)methyl>pyrrolidinylphosphonic triamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 60261-46-3
(2S)-2-[(diphenylphosphino)methyl]pyrrolidine

: 1605-65-8
N,N,N',N'-Tetramethylphosphorodiamidic chloride

: 145818-30-0
(S)-(-)-N,N,N',N'-tetramethyl-2-<(diphenylphosphino)methyl>pyrrolidinylphosphonic triamide

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1016/S0040-4020(99)00095-2

Reference yield:

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 145818-30-0
(S)-(-)-N,N,N',N'-tetramethyl-2-<(diphenylphosphino)methyl>pyrrolidinylphosphonic triamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium / 1) dioxane, reflux, 6 h; 2) THF, dioxane, rt, 1 h

2: 78 percent / trifluoroacetic acid / CH₂Cl₂ / 4 h / Ambient temperature

3: 79 percent / Et₃N / CH₂Cl₂

With sodium; triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/S0040-4020(99)00095-2

Reference yield:

: 145818-30-0
(S)-(-)-N,N,N',N'-tetramethyl-2-<(diphenylphosphino)methyl>pyrrolidinylphosphonic triamide

: 614-47-1
1,3-diphenyl-propen-3-one

: C₁₉H₂₅N₂O₂P

: C₁₉H₂₅N₂O₂P

Guidance literature:: With copper(l) iodide; methyllithium; In diethyl ether; at -20 ℃; for 1h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1039/c39930001248