3-acetamido-4-hydroxy-N,N-di-n-propylphenethylamine

Base Information

Chemical Name:3-acetamido-4-hydroxy-N,N-di-n-propylphenethylamine
CAS No.:101566-36-3
Molecular Formula:C₁₆H₂₆N₂O₂
Molecular Weight:278.395
Hs Code.:

Synonyms:3-acetamido-4-hydroxy-N,N-di-n-propylphenethylamine

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Chemical Property of 3-acetamido-4-hydroxy-N,N-di-n-propylphenethylamine

Chemical Property:

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Technology Process of 3-acetamido-4-hydroxy-N,N-di-n-propylphenethylamine

There total 9 articles about 3-acetamido-4-hydroxy-N,N-di-n-propylphenethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110925-48-9
N-[2-Benzyloxy-5-(2-dipropylamino-ethyl)-phenyl]-acetamide

: 101566-36-3
3-acetamido-4-hydroxy-N,N-di-n-propylphenethylamine

Guidance literature:: With hydrogen; ethyl acetate; palladium on activated charcoal; In methanol; under 3102.9 Torr;
DOI:10.1021/jm00156a010

Reference yield:

: 96886-46-3
4-(2-dipropylamino-ethyl)-phenol

: 101566-36-3
3-acetamido-4-hydroxy-N,N-di-n-propylphenethylamine

Guidance literature:: Multi-step reaction with 5 steps

1: 48 percent / aq. HNO₃ / acetic acid / Ambient temperature

2: K₂CO₃ / acetone / 2 h / Heating

3: HCl gas, H₂ / PtO₂ / methanol; diethyl ether / 3102.9 Torr

4: Ambient temperature

5: EtOAc, H₂ / 10percent Pd/C / methanol / 3102.9 Torr

With hydrogenchloride; hydrogen; nitric acid; potassium carbonate; ethyl acetate; platinum(IV) oxide; palladium on activated charcoal; In methanol; diethyl ether; acetic acid; acetone;
DOI:10.1021/jm00156a010

Reference yield:

: 142-84-7
di-n-propylamine

: 101566-36-3
3-acetamido-4-hydroxy-N,N-di-n-propylphenethylamine

Guidance literature:: Multi-step reaction with 8 steps

1: CHCl₃ / 2 h / 50 °C

2: diborane/THF / 4 h / Heating

3: 48percent aq. HBr / 4 h / Heating

4: 48 percent / aq. HNO₃ / acetic acid / Ambient temperature

5: K₂CO₃ / acetone / 2 h / Heating

6: HCl gas, H₂ / PtO₂ / methanol; diethyl ether / 3102.9 Torr

7: Ambient temperature

8: EtOAc, H₂ / 10percent Pd/C / methanol / 3102.9 Torr

With tetrahydrofuran; hydrogenchloride; hydrogen bromide; hydrogen; nitric acid; potassium carbonate; ethyl acetate; diborane; platinum(IV) oxide; palladium on activated charcoal; In methanol; diethyl ether; chloroform; acetic acid; acetone;
DOI:10.1021/jm00156a010