(Z)-3-(1,3-benzodioxol-5-yl)prop-2-en-1-ol

Base Information

Chemical Name:(Z)-3-(1,3-benzodioxol-5-yl)prop-2-en-1-ol
CAS No.:17581-86-1
Molecular Formula:C10H10 O3
Molecular Weight:178.18
Hs Code.:2932999099
NSC Number:15657
Mol file:17581-86-1.mol

Synonyms:NSC15657;(Z)-3-(1,3-benzodioxol-5-yl)prop-2-en-1-ol;NSC-15657;WLN: T56 BO DO CHJ G1U2Q;2-Propen-1-ol,3-benzodioxol-5-yl)-;2-Propen-1-ol,4-(methylenedioxy)phenyl]-

Suppliers and Price of (Z)-3-(1,3-benzodioxol-5-yl)prop-2-en-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
3'-HYDROXYISOSAFROLE 95.00%
5MG
$ 501.44

Total 5 raw suppliers

Chemical Property of (Z)-3-(1,3-benzodioxol-5-yl)prop-2-en-1-ol

Chemical Property:

Melting Point:78-78.8 °C
Boiling Point:340°Cat760mmHg
PKA:14.39±0.10(Predicted)
Flash Point:159.4°C
PSA：38.69000
Density:1.281g/cm³
LogP:1.42080
XLogP3:1.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:178.062994177
Heavy Atom Count:13
Complexity:191

Purity/Quality:

99% ^*data from raw suppliers

3'-HYDROXYISOSAFROLE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1OC2=C(O1)C=C(C=C2)C=CCO
Isomeric SMILES:C1OC2=C(O1)C=C(C=C2)/C=C\CO

Technology Process of (Z)-3-(1,3-benzodioxol-5-yl)prop-2-en-1-ol

There total 6 articles about (Z)-3-(1,3-benzodioxol-5-yl)prop-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 59901-90-5
(benzo[d][1,3]dioxol-5-yl)(oxiran-2-yl)methyl acetate

: 17581-86-1
3-(benzo[1,3]dioxol-5-yl)prop-2-en-1-ol

Guidance literature:: With bis(cyclopentadienyl)titanium (III) chloride; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

Reference yield:

: 14731-78-3
ethyl 3,4-methylenedioxycinnamate

: 17581-86-1
3-(benzo[1,3]dioxol-5-yl)prop-2-en-1-ol

Guidance literature:: With diisobutylaluminium hydride; In toluene; at -78 - 25 ℃; for 3.75h; Inert atmosphere;
DOI:10.1016/j.tetlet.2009.01.120

Reference yield:

: 120-57-0,30024-74-9
piperonal

: 17581-86-1
3-(benzo[1,3]dioxol-5-yl)prop-2-en-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 4 h / 80 °C

2: diisobutylaluminium hydride / dichloromethane / -20 °C

With diisobutylaluminium hydride; In dichloromethane; toluene;
DOI:10.3390/molecules16053580