1,1'-bis(diphenylvinylsilyl)ferrocene

Base Information

Chemical Name:1,1'-bis(diphenylvinylsilyl)ferrocene
CAS No.:862013-88-5
Molecular Formula:C₃₈H₃₄FeSi₂
Molecular Weight:602.706
Hs Code.:

Synonyms:1,1'-bis(diphenylvinylsilyl)ferrocene

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Chemical Property of 1,1'-bis(diphenylvinylsilyl)ferrocene

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Technology Process of 1,1'-bis(diphenylvinylsilyl)ferrocene

There total 1 articles about 1,1'-bis(diphenylvinylsilyl)ferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 102-54-5,55404-68-7
ferrocene

: 109-72-8,29786-93-4
n-butyllithium

: 110-18-9
N,N,N,N,-tetramethylethylenediamine

: 18419-53-9
vinyldiphenylchlorosilane

: 862013-88-5
1,1'-bis(diphenylvinylsilyl)ferrocene

Guidance literature:: In hexane; (Ar); placing of ferrocene, hexane and TMEDA into flask with stirring bar; addn. dropwise of soln. of n-BuLi in hexane, stirring for 20 h at room temp.; cooling to -78°C; treatment with SiClPh2(CH2CH) for 25 min; stirring for 8 h at room temp.; filtration, removal of excess solvent under vac., chromy. with silica using benzene/hexane as eluent; collection of second fraction, removal of solvent; elem. anal.;
DOI:10.1021/om050194x

Reference yield: 83.0%

: 862013-88-5
1,1'-bis(diphenylvinylsilyl)ferrocene

: 862013-90-9
(Z)-(1,1,4,4-tetraphenyl-1,4-disila-2,3-ethene)-[3]-ferrocenophane

Guidance literature:: carbonylchlorohydridobis(tricyclohexylphosphine)ruthenium(II); In toluene; (Ar); placing of RuH(Cl)(CO)(PCy3)2, Fe(C5H4SiPh2CHCH2)2 and toluene in minireactor with magnetic stirring; stirring and heating at 110°Cfor 18 h; removal of solvent under vac., repeated pptn. with cold pentane from toluene; elem. anal.;
DOI:10.1021/om050194x