(Z)-(1,1,4,4-tetraphenyl-1,4-disila-2,3-ethene)-[3]-ferrocenophane

Base Information

• Chemical Name: (Z)-(1,1,4,4-tetraphenyl-1,4-disila-2,3-ethene)-[3]-ferrocenophane
• CAS No.: 862013-90-9
• Molecular Formula: C₃₆H₃₀FeSi₂
• Molecular Weight: 574.652
• Mol file: 862013-90-9.mol

Synonyms:(Z)-(1,1,4,4-tetraphenyl-1,4-disila-2,3-ethene)-[3]-ferrocenophane

Chemical Property of (Z)-(1,1,4,4-tetraphenyl-1,4-disila-2,3-ethene)-[3]-ferrocenophane

Chemical Property:

Purity/Quality:

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Technology Process of (Z)-(1,1,4,4-tetraphenyl-1,4-disila-2,3-ethene)-[3]-ferrocenophane

There total 1 articles about (Z)-(1,1,4,4-tetraphenyl-1,4-disila-2,3-ethene)-[3]-ferrocenophane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

1,1'-bis(diphenylvinylsilyl)ferrocene (862013-88-5) → (Z)-(1,1,4,4-tetraphenyl-1,4-disila-2,3-ethene)-[3]-ferrocenophane (862013-90-9)

Guidance literature:

carbonylchlorohydridobis(tricyclohexylphosphine)ruthenium(II); In toluene; (Ar); placing of RuH(Cl)(CO)(PCy3)2, Fe(C5H4SiPh2CHCH2)2 and toluene in minireactor with magnetic stirring; stirring and heating at 110°Cfor 18 h; removal of solvent under vac., repeated pptn. with cold pentane from toluene; elem. anal.;

DOI:10.1021/om050194x

upstream raw materials:

1,1'-bis(diphenylvinylsilyl)ferrocene