1,13-dioxa-4,7,10,16,19,22-hexaaza-4,7,10,16,19,22-hexatosylcyclotetracosane

Base Information

Chemical Name:1,13-dioxa-4,7,10,16,19,22-hexaaza-4,7,10,16,19,22-hexatosylcyclotetracosane
CAS No.:83076-80-6
Molecular Formula:C₅₈H₇₄N₆O₁₄S₆
Molecular Weight:1271.65
Hs Code.:

Synonyms:1,13-dioxa-4,7,10,16,19,22-hexaaza-4,7,10,16,19,22-hexatosylcyclotetracosane

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Chemical Property of 1,13-dioxa-4,7,10,16,19,22-hexaaza-4,7,10,16,19,22-hexatosylcyclotetracosane

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Technology Process of 1,13-dioxa-4,7,10,16,19,22-hexaaza-4,7,10,16,19,22-hexatosylcyclotetracosane

There total 5 articles about 1,13-dioxa-4,7,10,16,19,22-hexaaza-4,7,10,16,19,22-hexatosylcyclotetracosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 83076-80-6
1,13-dioxa-4,7,10,16,19,22-hexaaza-4,7,10,16,19,22-hexatosylcyclotetracosane

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / pyridine / 5 h / 50 °C

2: 1.) sodium / 1.) CH₃OH, reflux, 2 h, 2.) DMF, 80 deg C, 1 h

With sodium; In pyridine;
DOI:10.1021/ja00387a030

Reference yield:

: 56187-04-3
1,4,7-tritosyl-1,4,7-triazaheptane

: 83076-80-6
1,13-dioxa-4,7,10,16,19,22-hexaaza-4,7,10,16,19,22-hexatosylcyclotetracosane

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / potassium carbonate / 72 h / 100 °C

2: 74 percent / pyridine / 4 °C

3: 1.) sodium / 1.) CH₃OH, reflux, 2 h, 2.) DMF, 80 deg C, 1 h

With sodium; potassium carbonate; In pyridine;
DOI:10.1021/ja00387a030

Reference yield:

: 83076-78-2
6,9,12-triaza-3,15-dioxa-6,9,12-tritosylheptadecane-1,17-diol

: 83076-80-6
1,13-dioxa-4,7,10,16,19,22-hexaaza-4,7,10,16,19,22-hexatosylcyclotetracosane

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / pyridine / 4 °C

2: 1.) sodium / 1.) CH₃OH, reflux, 2 h, 2.) DMF, 80 deg C, 1 h

With sodium; In pyridine;
DOI:10.1021/ja00387a030