benzyl-[3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-2-p-tolyl-allyl]-amine

Base Information

Chemical Name:benzyl-[3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-2-p-tolyl-allyl]-amine
CAS No.:878209-81-5
Molecular Formula:C₂₃H₃₀BNO₂
Molecular Weight:363.308
Hs Code.:

benzyl-[3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-2-<i>p</i>-tolyl-allyl]-amine

Synonyms:benzyl-[3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-2-p-tolyl-allyl]-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl-[3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-2-p-tolyl-allyl]-amine

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Technology Process of benzyl-[3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-2-p-tolyl-allyl]-amine

There total 2 articles about benzyl-[3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-2-p-tolyl-allyl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 865350-17-0
4,4,5,5-tetramethyl-2-(propa-1,2-dien-1-yl)-1,3,2-dioxaborolane

: 624-31-7
4-tolyl iodide

: 100-46-9
benzylamine

: 878209-81-5
benzyl-[3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-2-p-tolyl-allyl]-amine

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; trifuran-2-yl-phosphane; In toluene; react. boron compd. with amine and aryl iodide in the presence of palladium complex, phosphine and tertiary amine in toluene at 80°C for 24 h;
DOI:10.1021/ja057778a

Reference yield:

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 878209-81-5
benzyl-[3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-2-p-tolyl-allyl]-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 7.6 g / MgSO₄ / diethyl ether / 14 h / 20 °C

2: 71 percent / Pd₂(dba)3; P(2-furyl)3; i-Pr₂NEt / toluene / 24 h / 80 °C

With tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; trifuran-2-yl-phosphane; magnesium sulfate; N-ethyl-N,N-diisopropylamine; In diethyl ether; toluene;
DOI:10.1021/ja057778a

Reference yield:

: 878209-81-5
benzyl-[3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-2-p-tolyl-allyl]-amine

: 201230-82-2
carbon monoxide

: 1-benzyl-4-p-tolyl-1,5-dihydro-pyrrol-2-one

Guidance literature:: With palladium diacetate; triphenylphosphine; p-benzoquinone; In methanol; at 50 ℃; for 10h; atmospheric pressure;
DOI:10.1021/ja057778a