C₁₄H₁₁BrF₂

Base Information

Chemical Name:C₁₄H₁₁BrF₂
CAS No.:1188522-79-3
Molecular Formula:C₁₄H₁₁BrF₂
Molecular Weight:297.142
Hs Code.:

C<sub>14</sub>H<sub>11</sub>BrF<sub>2</sub>

Synonyms:C₁₄H₁₁BrF₂

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Chemical Property of C₁₄H₁₁BrF₂

Chemical Property:

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Technology Process of C₁₄H₁₁BrF₂

There total 6 articles about C₁₄H₁₁BrF₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1188522-77-1
C₁₄H₁₁BrF₂O

: 1188522-79-3
C₁₄H₁₁BrF₂

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;

Reference yield:

: 4122-56-9
methyl o-formylbenzoate

: 1188522-79-3
C₁₄H₁₁BrF₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: diethylamino-sulfur trifluoride / methanol / dichloromethane / 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

2.2: -78 °C / Inert atmosphere

3.1: tetrahydrofuran; diisobutyl ether / 1 h / -78 °C / Inert atmosphere

4.1: N-Bromosuccinimide / tetrachloromethane / 15 h / Inert atmosphere; UV-irradiation; Reflux

5.1: lithium aluminium tetrahydride / tetrahydrofuran / -78 °C / Inert atmosphere

5.2: Saturated solution

6.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / -78 - 20 °C / Inert atmosphere

With triethylsilane; N-Bromosuccinimide; lithium aluminium tetrahydride; n-butyllithium; diethylamino-sulfur trifluoride; boron trifluoride diethyl etherate; methanol; In tetrahydrofuran; tetrachloromethane; dichloromethane; diisobutyl ether;

Reference yield:

: 1188475-55-9
(2-(difluoromethyl)phenyl)(phenyl)methanone

: 1188522-79-3
C₁₄H₁₁BrF₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide / tetrachloromethane / 15 h / Inert atmosphere; UV-irradiation; Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran / -78 °C / Inert atmosphere

2.2: Saturated solution

3.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / -78 - 20 °C / Inert atmosphere

With triethylsilane; N-Bromosuccinimide; lithium aluminium tetrahydride; boron trifluoride diethyl etherate; In tetrahydrofuran; tetrachloromethane; dichloromethane;